Name Date Sect. Data Report Sheet: Quantitative Analysis of Group III Cations 21 Unknown # Draw the flow chart for this experiment and record you observations for each step. Use two different colors to record your observations from the known and the unknown. Ions Present in Unknown:

Chemical Principles in the Laboratory
11th Edition
ISBN:9781305264434
Author:Emil Slowinski, Wayne C. Wolsey, Robert Rossi
Publisher:Emil Slowinski, Wayne C. Wolsey, Robert Rossi
Chapter36: Qualitative Analysis Of Group I Cations
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Problem 1ASA
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Name
Date
Sect.
Data Report Sheet: Quantitative Analysis of Group III Cations
Unknown # 2
Draw the flow chart for this experiment and record you observations for each step.
Use two different colors to record your observations from the known and the unknown.
Ions Present in Unknown:
Transcribed Image Text:Name Date Sect. Data Report Sheet: Quantitative Analysis of Group III Cations Unknown # 2 Draw the flow chart for this experiment and record you observations for each step. Use two different colors to record your observations from the known and the unknown. Ions Present in Unknown:
UNKNOWN:
21
Sample
6 M NaOH
Boil
M NCIO
Boil
6 M NH.OH
Boil
Liquid
Solid
6 M CH,O,H
Until Acidic
M NH,OH
Discard tiquid
6 M NH.OH
Precipitate
Sof
6 M HNO,
Dissolve
Liquid
Solid
1 M BaCl,
Boil
6 M C,H.O.H
Dissolve
6 M NH.OH
Precipitate
Liquid
Solid
Catechol-
Violet
Dimethyl -
glyoxime
Discard
Solid
Liquid
6 M HNO,
Dissolve
6 M HCI
Dissolve
Reference:
Blue Solution:
AP-
Sample.
ClearSolution:
Refenence:
Red/Pink
Precipitate:
Sample.
Red/Pink
3% H,O,
Precipitate:
0.5 M
KSCN
Reference:
Sample.
Clear
Fading Blue
Solution:
Solution:
Reference:
Orange
Solution:
Fe
Sample.
Orange
Solutlon:
Fe
Transcribed Image Text:UNKNOWN: 21 Sample 6 M NaOH Boil M NCIO Boil 6 M NH.OH Boil Liquid Solid 6 M CH,O,H Until Acidic M NH,OH Discard tiquid 6 M NH.OH Precipitate Sof 6 M HNO, Dissolve Liquid Solid 1 M BaCl, Boil 6 M C,H.O.H Dissolve 6 M NH.OH Precipitate Liquid Solid Catechol- Violet Dimethyl - glyoxime Discard Solid Liquid 6 M HNO, Dissolve 6 M HCI Dissolve Reference: Blue Solution: AP- Sample. ClearSolution: Refenence: Red/Pink Precipitate: Sample. Red/Pink 3% H,O, Precipitate: 0.5 M KSCN Reference: Sample. Clear Fading Blue Solution: Solution: Reference: Orange Solution: Fe Sample. Orange Solutlon: Fe
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