On shaking a binary mixture in a separatory funnel, an emulsion is formed; briefly describe three methods by which you can break the emulsion.
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On shaking a binary mixture in a separatory funnel, an emulsion is formed; briefly describe three methods by which you can break the emulsion.
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- 2c）Outline a method based on extraction techniques for the separation of a mixture of compound B from problem I., and compound A from problem II.Which of the following would LOWER the purity of the distillate collected from the rubbing alcohol mixture? Using cold water in the condenserII. Not discarding the first milliliter distilledIII. Addition of boiling chips into the mixtureIV. Maintaining the temperature of the hot plate above 100°C Select one: I and II III and IV II and IV II onlyYou were given a mixture of two miscible solvent A and B that you are tasked to separate. You know that solvent A has a boiling point of 49 oC while solvent B has a boiling point of 174 oC. Which of the listed method would overall be the most efficient? Fractional distillation Recrystallization Solid-liquid extraction Liquid-liquid extraction Simple distillation Acid-Base extraction
- Transfer 3-4 drops or a pinch of the test compound (Acetanilide) to 3 ml of the solvents, 5% NaOH and 5% HCL Shake the mixture thoroughly. The time required for the solute to dissolve in the solvent should not be more than 2 minutes. Indicate with (+) or (-) if the test compound is soluble or insoluble in the solvent. What is the solubility class of Acetanilide in 5% NaOH? (Very soluble, freely soluble, soluble, sparingly soluble, slightly soluble, very slighlty soluble, practically insoluble) What is the solubility class of Acetanilde in 5% HCL? (Very soluble, freely soluble, soluble, sparingly soluble, slightly soluble, very slighlty soluble, practically insoluble)the eugenol and water distillate you collect is apt to be cloudy, particularly the first part of this distillate. Explain why.Transfer 3-4 drops or a pinch of the test compound (Acetanilide) to 3 ml of the solvents, 5% NaOH and 5% NaHCO3 Shake the mixture thoroughly. The time required for the solute to dissolve in the solvent should not be more than 2 minutes. Indicate with (+) or (-) if the test compound is soluble or insoluble in the solvent. What is the theoretical solubility of Acetanilide in 5% NaOH? _______ What is the theoretical solubility of Acetanilide in 5% NaHCO3? _______
- 6.0 mL of cyclohexanol, 8 mL of 85% phosphoric acid, and 10 drops of sulfuric acid are added to a 50-mL round-bottom flask with boiling chips, and the mixture is distilled into an ice-cooled receiver. The distillate is in the form of a colorless bi-phasic mixture. The cyclohexene upper layer is removed from the water layer, and dried over anhydrous calcium chloride. Isolated is cyclohexene as a clear and colorless foul-smelling liquid. Weighing data is given below. Gross mass: 51.24 g Tare mass: 48.04 g Product mass: 3.2g Question: Calculate the theoretical mass of the cyclohexene product, bearing in mind that the cyclohexanol starting material was measured by volume, not by mass (so you must use the density of cyclohexanol to convert milliliters to grams, before calculating the number of moles). Calculate the percent yield of cyclohexene obtained.The separation and purification processes given below and the method used against them are given. Which or which of these pairings are correct? I. Brewing of tea - ExtractionII. Purification of water impurities - ChromatographyIII. Separating olive pomace from olive oil while producing olive oil-DecantationIV.Petroleum fractions obtaining - Ordinary distillationV. Obtaining essential oils and using them in perfume making - Water-steam distillationA. I, II, III, IVB. I, II, III, IV, VC. I, IV, VD. I, II, III, VE. I, II, VTransfer 3-4 drops or a pinch of the test compound (Acetanilide) to 3 ml of the solvents, 5% NaOH and 5% HCL Shake the mixture thoroughly. The time required for the solute to dissolve in the solvent should not be more than 2 minutes. Indicate with (+) or (-) if the test compound is soluble or insoluble in the solvent. Is Acetanilide solube or insolube in 5% NaOH? _______ Is Acetanilde soluble or insolube in 5% HCL? _______
- 1,4‐Dimethoxybenzene (0.642 g) was dissolved in 2.0 mL acetic acid in a 25 mL Erlenmeyer flask using heat from a hot plate. Once the solid dissolved, 1.0 mL tert‐ butanol was added, and the reaction mixture was cooled in an ice bath. Then 2.0 mL concentrated sulfuric acid was added in 2‐3 drop portions,stirring the mixture after each aliquot. After the addition, the flask was removed from the ice bath and allowed to sit at room temperature for 15 minutes. Then 1.0 mL water was added dropwise to dilute the acid and the reaction mixture was added to 40 mL cold water in a 100 mL beaker. The solid was vacuum filtered and washed with 5 mL cold water, giving 52 g filtrate. The product wasrecrystallized from 4.5 mL methanol, yielding 0.317 g purified 1,4‐di‐tert‐butyl‐2,5‐dimethoxy benzene (27.2% yield). What is the atom economy, e-factor, and effective mass yield?Why is the titration done with vigorous swirling?Standard solution : 0.201 grams of acetylsalicylic acid was combined with 10 mL of 0.5 M NaOH, then transfered to a 100 mL flask and filled the rest of the way with water Then 0.500 mLs of the standard solution was transfered to a 10.00 mL flask and diluted to the 10 mL mark with 0.02 M of buffered iron chloride. This step was repeated using 0.400, 0.300, 0.200, 0.100 mLs of the standard solution Questions: A.) determine the concentration of the acetylsalicylic acid in the 100.00 mL volumetric flask containing the solution from which the standards were made. B.)determine the concentration of the acetylsalicylic acid in each of the 10.00 mL calibration solutions. I only need the work for 0.400 mLs C.)Make a scatter plot (on the computer again) of absorbance versus concentration for the calibration samples. On the plot, add a linear trendline, and display the equation and the R2 value on the chart. Take your time to label the axes
