Phena Cetin 80 75 70 65 60 55 45 40 35 30 25 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1) %Transmittance 3285.28 3256.85 3189.85 3132.99 3082.23 2986.80 2925.89 2887.31 2860.91 1658.88 1553.30 1610.15 1510.66

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter7: Components Of Optical Instruments
Section: Chapter Questions
Problem 7.8QAP
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Can you answer this question please according to the prodecure and IR graph

Please talk and describe all the details in the IR graph and how pure our substance was accoring to the IR graph 

1.063 g of p-acetamidophenol was measured out into a 50 mL round bottom flask along with 8 mL of 1M NaOH in ethanol and a stir bar. This mixture was heated at reflux for 15 min. It was allowed to cool and then 0.80 mL of bromoethane was added to the reaction. The mixture was then heated at reflux for another 15 min. After heating, the solution was poured onto a mixture of ice and water and further cooled on ice and then the solid was collected by vacuum filtration. This solid was then recrystallized from ethanol and water. The final mass of the purified phenacetin was 0.42250 g 

 

Phenacetin
80
75
70
65
60
55
50
45
40
35
30
25
4000
3500
3000
2500
2000
1500
1000
500
Wavenumbers (cm-1)
%Transmittance
3285.28
3256.85
3189.85
3132.99
3082.23
2986.80
2925.89
2887.31
2860.91
1658.88
1553.30
1610.15
1510.66
Transcribed Image Text:Phenacetin 80 75 70 65 60 55 50 45 40 35 30 25 4000 3500 3000 2500 2000 1500 1000 500 Wavenumbers (cm-1) %Transmittance 3285.28 3256.85 3189.85 3132.99 3082.23 2986.80 2925.89 2887.31 2860.91 1658.88 1553.30 1610.15 1510.66
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