Please provide a structure consistent with the following IR, 13C NMR, and 1H NMR spectra. Assign at least two bands in the IR and assign all protons in the 1H NMR/13C NMR spectrum. Show calculation of degree of unsaturation and explain your reasoning.

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter26: An Introduction To Chromatographic Separations
Section: Chapter Questions
Problem 26.15QAP
icon
Related questions
Question
Please provide a structure consistent with the following IR, 13C NMR, and 1H NMR spectra. Assign at least two bands in the IR and assign all protons in the 1H NMR/13C NMR spectrum. Show calculation of degree of unsaturation and explain your reasoning.
20-
40-
60-
80-
Problem 6
Formula: CsH1002
100
2984
2945
1740
4000
3500
3000
2500
2000
1500
2H
3.5
2H
1192
1833-
1000
3H
|зн
3.0
2.0
1.0 PPM
Transcribed Image Text:20- 40- 60- 80- Problem 6 Formula: CsH1002 100 2984 2945 1740 4000 3500 3000 2500 2000 1500 2H 3.5 2H 1192 1833- 1000 3H |зн 3.0 2.0 1.0 PPM
28-
40
68-
Problem 5
Formula: CsH13N
100-
12-99CC
2983.2922.76.23-
4800
3508
3000
2500
2000
1500
1H
2H 2H
2H
6H
T
4.0
3.5
3.0
2.5
2.0
1.5
1.0
0.5 PPM
600.04
1462.23-
1377.35
1000
10:21
1149.72-
1045.55
Transcribed Image Text:28- 40 68- Problem 5 Formula: CsH13N 100- 12-99CC 2983.2922.76.23- 4800 3508 3000 2500 2000 1500 1H 2H 2H 2H 6H T 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 PPM 600.04 1462.23- 1377.35 1000 10:21 1149.72- 1045.55
Expert Solution
steps

Step by step

Solved in 3 steps with 2 images

Blurred answer
Knowledge Booster
Mass Spectrometry
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Recommended textbooks for you
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Fundamentals Of Analytical Chemistry
Fundamentals Of Analytical Chemistry
Chemistry
ISBN:
9781285640686
Author:
Skoog
Publisher:
Cengage