Question 4 Packing a capillary tube loosely with the sample will not impact the melting point analysis True False Question 5 Diethyl ether (DEE) is used during the Grignard synthesis because DEE is a polar protic solvent O DEE is a non-polar solvent O DEE is a polar aprotic solvent DEE generates required nucleophile

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter4: Recrystallization
Section: Chapter Questions
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Solve all threes please...
Question 4
Packing a capillary tube loosely with the sample will not impact the melting point analysis
True
False
Question 5
Diethyl ether (DEE) is used during the Grignard synthesis because
DEE is a polar protic solvent
O DEE is a non-polar solvent
O DEE is a polar aprotic solvent
DEE generates required nucleophile
Transcribed Image Text:Question 4 Packing a capillary tube loosely with the sample will not impact the melting point analysis True False Question 5 Diethyl ether (DEE) is used during the Grignard synthesis because DEE is a polar protic solvent O DEE is a non-polar solvent O DEE is a polar aprotic solvent DEE generates required nucleophile
Question 3
During Grignard synthesis experiment, the Mg powder is grinded in the test tubę using a glass
rod for
breaking Mg metal into fine powder
O Activating the Mg metal
for solubilizing the Mg metal in diethyl ether
For all above reasons
Transcribed Image Text:Question 3 During Grignard synthesis experiment, the Mg powder is grinded in the test tubę using a glass rod for breaking Mg metal into fine powder O Activating the Mg metal for solubilizing the Mg metal in diethyl ether For all above reasons
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