Upon running a standard recrystallization in 90:10 EtOH:water you reach a point where crystals are not forming! You get very nervous as everyone else is getting excellent crystal formation. Which of the following would be an appropriate response? O Gently scratch the glass vessel with a glass stir rod to induce crystallization. O Add additional solvent to the vessel. Additional solvent will help reduce the solubility of the solid. O Stir the liquid on a stir plate with a stir bar to induce crystallization. O Dump the material in the waste, there isn't any hope at this point.
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- MAKE A FLOWCHART/SCHEMATIC DIAGRAM Procedure: Place 20 drops of each of 0.2M CuSO4 in a centrifuge tube. Then add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Record your observation. Centrifuge the mixtures for 3 mins. and decant the supernatant liquid. Add 10 drops of DI water and 10 drops of 6M HNO3. Stir and boil the mixture in a hot water bath for 5 mins. centrifuge the mixture for 3 mins. Decant the supernatant solution from procedure 3. Discard the To each of the supernatant liquid, add 6 drops of 6M H2SO4. Allow themixtures to cool and 5 drops of DI water. To the mixtures in procedure 4, add few drops of concentrated NH3 until the solution becomes basic. Confirm using a litmus paper. Record your observation. Add 1 drop of 5M NaOH and 1 drop of 0.1 M SnCl2 to the centrifuge tube containing Bi3+ ion , centrifuge and decant the supernatant liquid. To the solution containing Sn 2+ion , add 6M HCl , dropwise in the test tube. Stir well. Add excess HCl in the…When isolating the solid after recrystallization using vacuum filtration what solvent should you use to aid in the rinse from the Erlenmeyer flask to the vacuum filter funnel? (Only pick one answer) Group of answer choices: Cold ethyl acetate Cold ethanol Hot ethyl acetate Hot ethanol Hot water Cold water None of the above, it should not be risnedExplain whether each of the following is a source of experimental error: a. He transfers the stir bar straight from flask #1 to flask #2 without washing or rinsing it. b. He washes and rinses the flasks but again does not dry them before pipetting the vinegar into each.
- Based on the melting point of your impure solid, you look at the given samples and believe you havecompound A. Compound A is recrystallized using a mixed solvent system of ethanol and water. You add1 ml of hot ethanol to your sample and it doesn’t completely dissolve. You continue to add hot ethanolbut there isn’t any change. Some solid remains. What should you do next?The best liquid mixtures for separation by simple distillation need to have boiling points that differ by at least ___________ oC. 10 20 30 4010g coffee 4g sodium carbonate 40m dichloromethane 160ml distilled water coffee filter What are the principles behind caffeine being extracted from coffee using the above items? 1st sodium carbonate mixed with coffee then brought to a boil for 20min then solution/grinds are filtered. Then solution is added to a separatory funnel with 15ml of dichloromethane and two layers are observed so the bottom layer with DCM contains the caffeine, then this layer is collected in a beaker and dried out using molecular seeds. Then the solvent is brought to a boil with crude caffeine remaining and recystallized using 95% ethanol and brought to a boil again. Then the contents are vaccum filtered and allowed to dry resulting in 30mg caffeine.
- 4.0g of potassium hydrogen tartrate was added to 300mL distilled water. The temperature of the solution is 23.1C. The liquid was filtered and 50mL of the filtered solution was transferred to 250mL beaker, two drops of phenolpthalein was added to the 250mL beaker. The concentration of NaOH is 1.0 M that is filled in the 2mL graduate pipette, single drops of NaOH was added to the 250mL beaker until the solution turns pink and the potassium hydrogen tartrate reach the endpoint. The datd of four trials was collected. Please answer the following questions 4) calculate ksp for potassium hydrogen tartrate for each trial and average ksp for thr experiment 5) calculate the percent error in you value of ksp using reference that is found as the theoretical value. 6) why was the temperature of the saturated solution recorded?4.0g of potassium hydrogen tartrate was added to 300mL distilled water. The temperature of the solution is 23.1C. The liquid was filtered and 50mL of the filtered solution was transferred to 250mL beaker, two drops of phenolpthalein was added to the 250mL beaker. The concentration of NaOH is 1.0 M that is filled in the 2mL graduate pipette, single drops of NaOH was added to the 250mL beaker until the solution turns pink and the potassium hydrogen tartrate reach the endpoint. The datd of four trials was collected. Please answer the following questions 1) calculate the total volume and moles of NaOH required to reach the endpoint for each trial. 2) calculate the molar solubility of potassium hydrogen tartate ( in mol/L) for each trial. 3) calculate the average molar solubility of potassium hydrogen tartate for the four trials. What is the average solubility of potassium hydrogen tartrate in g/L? 4) calculate ksp for potassium hydrogen tartrate for each trial and average ksp for thr…How can you tell that a compound is impure? (or pure?) What are the characteristics considered when taking a melting point? What is recrystallization? What is happening on a molecular level (videos are provided) How are solvents chosen for recrystallization? (single solvent or mixed-solvent system).What are the properties of a good solvent system? How are crystals collected?
- is water a good solvent for recrystallization for acetanilide based on the image?. The total cation content of natural water is often determined by exchanging the cations for hydrogen ions on an ion exchange resin. The cations are adsorbed to the resin which releases H+ (1:1 exchange) which can then be titrated with a base. A 25.0 mL sample of a natural water is diluted to 100 mL with distilled water and 2.0 g of a cation-exchange resin was added. After stirring, the mixture was filtered and the solid remaining on the filter paper was washed with three 15.0 mL portions of distilled water. The filtrate and washing required 15.3 mL of 0.0202 M NaOH to reach the equivalence pt. Calculate the number of moles of cation present in 1.00 L of sample.Matt was heating his methanol solvent in an E. flask on a hot plate to use for recrystallization. The TAcame by and noticed he didn’t have a stir stick or boiling chip in the flask and told him to use one,please. Matt dropped a stick in the flask and suddenly the liquid exploded out of the flask. Oops! Tellme why that happened. What should he have done instead?