Upon running a standard recrystallization in 90:10 EtOH:water you reach a point where crystals are not forming! You get very nervous as everyone else is getting excellent crystal formation. Which of the following would be an appropriate response? O Gently scratch the glass vessel with a glass stir rod to induce crystallization. O Add additional solvent to the vessel. Additional solvent will help reduce the solubility of the solid. O Stir the liquid on a stir plate with a stir bar to induce crystallization. O Dump the material in the waste, there isn't any hope at this point.

Organic Chemistry
9th Edition
ISBN:9781305080485
Author:John E. McMurry
Publisher:John E. McMurry
Chapter31: Synthetic Polymers
Section31.SE: Something Extra
Problem 28AP
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Upon running a standard recrystallization in 90:10 EtOH:water you reach a point where crystals are
not forming! You get very nervous as everyone else is getting excellent crystal formation. Which of
the following would be an appropriate response?
O Gently scratch the glass vessel with a glass stir rod to induce crystallization.
Add additional solvent to the vessel. Additional solvent will help reduce the solubility of the solid.
Stir the liquid on a stir plate with a stir bar to induce crystallization.
O Dump the material in the waste, there isn't any hope at this point.
Transcribed Image Text:Upon running a standard recrystallization in 90:10 EtOH:water you reach a point where crystals are not forming! You get very nervous as everyone else is getting excellent crystal formation. Which of the following would be an appropriate response? O Gently scratch the glass vessel with a glass stir rod to induce crystallization. Add additional solvent to the vessel. Additional solvent will help reduce the solubility of the solid. Stir the liquid on a stir plate with a stir bar to induce crystallization. O Dump the material in the waste, there isn't any hope at this point.
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