Vaccum filtration is the major technique used in this experiment. The following step sequences are recommended: 1) turn on vacuum 2) wet the filter paper and 3) pour the product solution into the buchner funnel. can the Vacuum be turned on in the last step instead?explain
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Vaccum filtration is the major technique used in this experiment. The following step sequences are recommended: 1) turn on vacuum 2) wet the filter paper and 3) pour the product solution into the buchner funnel.
can the Vacuum be turned on in the last step instead?explain
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- A student doing this experiment had some problems with the procedure, as described below. Explain what effect each problem would have had on the magnitude of the results calculated. b) The student neglected to open the pinch clamp on the plastic tubing between the filter flask and the beaker when the Mg came in contact with the HCl solution. After the stopper popped out of the Erlenmeyer flask, the student quickly replaced the stopper, opened the clamp, and proceeded with the experiment. c) The student began titrating the unreacted HCl with standard NaOH solution and realized that there was a large air bubble in the buret tip. The bubble came out as the first few milliliters of titrant were added. d) The student forgot to add indicator to the titration mixture until 12.50 mL of titrant had been added. When the indicator was finally added, the solution was colorless.Why is it not necessary to dry the Erlenmeyer flask between each trial?Why is the final product from recrystallization isolated by vacuum filtration and not by gravity filtration?
- What is the other term for mobile phase in chromatography? (Eluant, Eluate, or Solvent)In vacuum filtration, the filter paper should be wet before the final product solution is poured into the buchner funnel. Explain why such an action should be implemented.A student properly sets up a column chromatography experiment. Although the mixture is soluble in the mobile phase, the sample appears "stuck" at the top of the column and will not elute regardless of how much solvent is applied. What could be the cause of this problem and what could the student do to try and achieve a successful separation?
- The following questions relate to the column chromatography experiment.a. Why does the fluorene elute first from the column?b. Why was the solvent changed in the middle of the column procedure?What is the role of the moist filter paper inside the developing chamber during a Thin-Layer Chromatography Experiment?Of Aspirin, ethanol, acetaminophen, ethyl acetate, hexane, and water which could go undetected during HPLC analysis, but could result in a lower than expected melting point, why are they not detected by HPLC analysis?
- If insoluble impurities, e.g., dust, tissue, filter paper, etc., were mixed with the sample, how would these affect the measured melting point?Briefly explain the reasons for the use of the following techniques in this experiment. a. The hydrate salt is heated with the crucible cover in an ajar position rather than in a fully seated position or having the crucible completely uncovered. b. The crucible cover is fully seated during cooling and weighing of the residue.In this experiment, you will be performing TLC on your 'crude' and 'recrystallized' biphenyl samples. How many spots would you expect to see in each lane? Explain your answer. 2. If you perform pipette (column) chromatography on the mixture containing biphenyl and organic dye, which compound would you expect to elute from the column last. Explain your answer.