What is the IR and HNMRAndCNMR and mass and mass in this example

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter20: Molecular Mass Spectrometry
Section: Chapter Questions
Problem 20.11QAP
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What is the IR and HNMRAndCNMR and mass and mass in this example
10
IR Spectrum
(liquid film)
L
4000
ملفلمسلسلام
100
80
60
405 ㅎ
20
40
13C NMR Spectrum
(20.0 MHz. CDCI, solution)
off-resonance decoupled
proton decoupled
200
'H NMR Spectrum
(100 MHz, CDCI, solution)
% of base peak
при
9
3000
77
80
1
105
120
u
8
2000
1690
v (cm¹)
M
134
160
m/e
7
160
1600
6
200
120
1200
800
Mass Spectrum
240
5
сл
C₂H100
280
solvent
80
4
0.0
0.5
1.0
1.5
Problem 30
UV spectrum
1.075 mg/10 mls
path length: 0.10 cm
solvent ethanol
300
λ (nm)
lle
absorbance
200
3
40
250
2
0
1
350
8 (ppm)
TMS
0
8 (ppm)
119
Transcribed Image Text:10 IR Spectrum (liquid film) L 4000 ملفلمسلسلام 100 80 60 405 ㅎ 20 40 13C NMR Spectrum (20.0 MHz. CDCI, solution) off-resonance decoupled proton decoupled 200 'H NMR Spectrum (100 MHz, CDCI, solution) % of base peak при 9 3000 77 80 1 105 120 u 8 2000 1690 v (cm¹) M 134 160 m/e 7 160 1600 6 200 120 1200 800 Mass Spectrum 240 5 сл C₂H100 280 solvent 80 4 0.0 0.5 1.0 1.5 Problem 30 UV spectrum 1.075 mg/10 mls path length: 0.10 cm solvent ethanol 300 λ (nm) lle absorbance 200 3 40 250 2 0 1 350 8 (ppm) TMS 0 8 (ppm) 119
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