What is the IR and HNMRAndCNMR and mass

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter19: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 19.36QAP: From the proton NMR spectrum in Figure 19-44, deduce the structure of this hydrocarbon
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What is the IR and HNMRAndCNMR and mass
4000
dadadadadada
% of base peak
80
13C NMR Spectrum
DEPT ou out out
proton decoupled
200
H NMR Spectrum
(400 MHz, CDC, solution)
10
9
m
1600
1200
8
2000
V tom
117
120 160
m/e
expansion
expansion
130 129 ppm
160
7
200
120
6
800
Mass Spectrum
C₂H-N
290
240
5
80
4
Problem 25
40
3
2
0
1
8 (ppm)
TMS
L
0
8 (ppm
Transcribed Image Text:4000 dadadadadada % of base peak 80 13C NMR Spectrum DEPT ou out out proton decoupled 200 H NMR Spectrum (400 MHz, CDC, solution) 10 9 m 1600 1200 8 2000 V tom 117 120 160 m/e expansion expansion 130 129 ppm 160 7 200 120 6 800 Mass Spectrum C₂H-N 290 240 5 80 4 Problem 25 40 3 2 0 1 8 (ppm) TMS L 0 8 (ppm
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