What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a redox titration? and why is back titration used? 2. What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a precipitation titration? and why is back titration used? 3. What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a complexometric titration? and why is back titration used?

What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a redox titration? and why is back titration used? 2. What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a precipitation titration? and why is back titration used? 3. What is the Sample, Analyte, Reagent added in excess, and Reagent used in an example of back titration in a complexometric titration? and why is back titration used?

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

ChapterA1: Evaluation Of Analytical Data

Section: Chapter Questions

Problem A1.23QAP

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This is an unknown solution which comprises of several ions possible for analysis. From the given information, determine which ions are present. Use + for positive, - for negative, or ? for insufficient information. An unknown solution containing the ions listed to the right was found: For Group I Cations: 1). A white precipitate was generated when 2 drops of 6M HCl solution was added to the unknown solution test tube. 2). Di water was added to the solution from part 1, and then the ppt was separated from the supernatant. The ppt was then washed with DI water few times to make sure is ppt is clean. 3). On the ppt separated from part 2 excess 6M NH3 was added and as a result all the ppt was dissolved. For Group III Cations: 4). An addition of Excess 6M NH3 led to a basic solution and a ppt. The ppt was then separated from the supernatant. 5). When Excess 6M NaOH was…
For titration, what is the purpose of a dropwise rate?
1. How does calculation of the electrode potential of the system at the equivalence point differ from that for any other point of an oxidation/reduction titration?
A. What is the characteristic color of ferric ions in solution? B. Why is the titration of the oxalate in the green salt with KMnO4 performed prior to carrying out the redox titration for iron content? (Why can’t you do them the other way – iron first then oxalate?) C. In a titration using 0.02000 M KMnO4 solution, the following data were obtained: Buret readings: FINAL = 15.31 mL INITIAL = 5.02 mL How many moles of KMnO4 were used?
Explain the half drop titration technique
Show complete solution. Round-off your answers to four decimal places The amount of copper in a wire was determined by a redox titration using KMnO4 as the titrant. A 0.4185-g sample was dissolved in acid and the liberated Cu2+ quantitatively reduced to Cu+, using a reductor column. Titrating with 0.0250 M KMnO4 requires 41.27 mL to reach the endpoint. Determine the % w/w CuO in the sample of meteorite. Answer: % CuO = ______
Calculations for Acetate Buffer Solutions Molarity of acetic in acetate buffer (below is the data to answer the answer) Deionized water Acetate Buffer Ammonia Buffer pH of solution 6.62 4.59 9.49 Ph of solution after addition of 1 mL of 0.6 M NaOH 12.41 4.71 9.50 pH of solution after addition of 1 mL of 0.6 M HCl 1.38 3.87 9.24 Preparation of Buffer solutions Mass of sodium acetate in acetate buffer ~ 1.1981 Volume of 3.0 M acetic acid in acetate buffrer ~ 3.81 Mass of ammonium chloride ~ 1.2721 Volume of 5.0 M NH4OH ~ 6.00
The following glassware is used when we do titrimetric analysis. If the glassware is not fully dry when used (i.e., there is water left in the glassware), determine whether this will affect the results of the titration process. Give a brief explanation. a. Erlenmeyer flask (used during titration) b. Burette c. Pipet (used in transferring the sample) d. Volumetric flask
Shana, a student in the Analytical Chemistry class, performed a Redox Titration to determine the content of hypochlorite ions (% w/w) in an unknown solution. First, Shana prepared a primary standard solution of KIO3 by dissolving 0.4791 g dry KIO3 in 250.00 mL DI water. Next, using the procedure in your lab manual, Shana used 50.00 mL of this primary standard solution to standardize the Na2S2O3 titrant, and 26.25 mL of titrant was consumed. Next, Shana prepared the unknown solution by diluting 12.8624 g of the solution in 250.00 mL of DI water. A 50.00 mL portion of this dilute unknown solution was titrated using the procedure in your lab manual, and 19.25 mL of Na2S2O3 solution was consumed. Answer the following questions about this titration. Recall the stoichiometry of the NET chemical equation for this reaction. Note: use appropriate significant figures in your answer! A. Calculate the concentration (M) of Na2S2O3 titrant. B. Determine the amount (g) of hypochlorite ion in 50.00 mL…
6. Why do we need to precipitate from a hot solution? 7. Why is the precipitating agent added all at once? 8. What is the purpose of adding 6M HCI in the sample solution? 9. Why do we need to test the washings with AgNO3? 10. What is done in an ignition process? 11. What is the product after the precipitate was ignited? 12. What are the advantages of performing ignition? 13. Cite the sources of errors for this experiment and explain how to possibly circumvent these kinds of problems.
Which statement is NOT correct? pH meter should always be standardized before using to make sure that your readings are accurate and repeatable. The electrode tips should never touch the bottom or sides of a beaker. When finished using the pH meter, rinse the electrode and place it in the pH 7 buffer solution on standby. One buffer solution is enough to standardize a pH meter before using.
Why are many ionic precipitates washed with electrolyte solution instead of pure water?