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- Write the appropriate distillation method in the blank of the statement below. i) Separation of components with similar boiling points is required a ...(a)... distillation.ii) Isolation of water-insoluble components often with high boiling points from plant materials is required a ...(b)... distillation.iii) Separation of components with very different boiling points is required a ...(c)... distillation.iv) Separation of components with high boiling points is required a ...(d)... distillation.Please answer the question at the bottom. Fractional distillation Measure 55 mL of 40% ethanol Place 50 mL of ethanol in your distilling flask taking care that no liquid enters the side arm. Place the remaining 5 mL of ethanol in a test tube and set aside for procedure 2. Add a few marble or porcelain chips to the distilling flask to prevent bumping. Bumping is a term given to irregular boiling Assemble the rest of the apparatus for a simple distillation set-up. You may ask assistance from your instructor Cover the top of the distilling flask with a cork fitted with a thermometer. Make sure that the tip of the thermometer bulb is just below the side arm of the distillation flask Check all connections for tightness Heat the contents of the flask to boiling. Adjust the flame when the sample is already boiling. Make sure that it does not boil to dryness. Note the temperature of the first drop. Collect 60 drops of distillate per test tube. You will need 5 test tubes, thus five…Define Distillation?
- Compare and contrast simple and steam distillation in terms of the type of mixtures separated by each technique.Purpose of the boiling stones during the distillation process is: a. avoid the formation of bubbles b. prevent overheating of the solution c.help the liquid heat up faster d. help separate the components of the mixtureWhen should you NOT use simple distillation? Two liquids with boiling points less than 30 °C apart. The liquid has no more than 10% liquid contaminants. One of the liquids is non-volatile. Two liquids with boiling points more than 30 °C apart.
- Are each of the following things good or bad in a distillation? (a) The distillation stops at one point, and the temperature drops. (b) The material in the distilling flask boils violently and some sloshes up and into the condenser (c) You forget to run water through the condenser. (d) Distillate drops out of the condenser at the rate of about one drop per second.A sample of crude oil undergoes fractional distillation with _____ being collected at the bottom of the distillation tower, and _____ at the top. a. Diesel and jet fuel; gasoline b. Gasoline; kerosene c. Methane and ethylene; diesel and jet fuel d. High molecular weight fractions; methane and ethylene e. Kerosene; high molecular weight fractionsA natural product (MW = 150) distills with steam at a boiling temperature of 99°C at atmospheric pressure. The vapor pressure of water at 99°C is 733 mmHg. Calculate the weight of natural product that co-distills with each gram (1 g) of water at 99°C.
- Chemicals AmountBenzophenone 0.523 g (2.87*10^-3mol)Sodium borohydride 0.12 g (3.2*10^-3 mol)Benzhydrol 0.357 g (1.94*10^-3mol)Observed melting point 65-66 degree C Theroretical yield of Benzophenone ________ Percent yield _______________ Theoretical melting point __________--Please answer both questions.1. Arrange the following steps based on the order they occur in a distillation process:I. The vapor condenses with the aid of flowing cold water in the condenserII. The liquid is collected in the receiving flask, removing the first 1 mL of the distillateIII. The mixture is heated in the distilling flask while simultaneously monitoring the temperatureIV. The more volatile component evaporates and passes through the three-way connector2. The components of an 80-mL rubbing alcohol sample were separated using distillation and the resulting percent recovery of isopropyl alcohol is 14.70%. Determine the volume, in mL, of isopropyl alcohol present in the sample. a. 11.86 mL b. 11.76 mL c. 11.23 mL d. 12.45 mLWhich of the following pairs of liquids could be separated by simple distillation? Why? a. Ethyl acetate (b.p. 77°C) & Phenol (b.p. 181.7°C) b. Cyclohexane (b.p. 80.7°C) & Toluene (b.p. 111C) C. Hexane (b.p. 69.10C) & Ethylbenzene (b.p. 136°C)