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- You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.You find that methylphenidate is highly soluble in 2-methyltetrahydrofuran, a bio-renewable solvent. Draw the structure of 2-methyltetrahydrofuran and give two reasons why it is a good solvent choice for liquid-liquid extraction.You are employed as a coop student at the Drug and Alcohol Testing Association of Canada (DATAC) developing analytical tests for sports doping agents. You are asked to prepare a procedure for the extraction of methylphenidate, the active compound in Ritalin, from urine samples (consider them as simple aqueous layers, you do not need to consider other components!). The goal of the procedure is to extract the methylphenidate into an organic layer which will then be evaporated, and the residue will be tested for the drug.Your colleague is helping you develop the urine test. They suggest that the urine should be adjusted to a pH above 7 before extracting with the organic solvent. Why is this necessary? Support your explanation with a full arrow-pushing mechanism for the reaction that would occur if the pH was below 7. Include all formal charges, intermediates (if applicable) and products.A chemist is asked to separate the components of a mixture composed of 1.00 g each of the two compounds shown below. The chemist has access to the following bases: 10% aqueous NaHCO3 and 10% aqueous NaOH. Which base and how many mLs of the base (i.e., the minimum amount) are needed to completely separate these compounds from each other by liquid-liquid extraction?
- Naphthalene, C10H8 is insoluble in water but sublimes easily when heated. How could you separate a mixture of naphthalene and NaCl? Suggest two different methods. asapSuppose you have a mixture of copper sulfate (CuSO4) and azulene (C10H8, you may wish to know the structure of azulene). Both copper sulfate and azulene are beautiful deep blue cystalline solids. If you transferred the mixture to a separatory funnel containing both an aqueous and and organic solvents (1M HCl and dichloromethane), into which layer would the copper sulfate partition, aqueous or organic? Aqueous layer (1M HCl) Organic layer (dichloromethane) Copper sulfate would partition nearly equally into both the aqueous and organic layersIsopropanol is a good extraction solvent for plant pigments as it breaks down cell walls and is miscible with pigments. Can you be sure that you only extracted chlorophyll-a from your spinach leaf? If not, what else might have been extracted?
- Describe in words and by means of complete chemical equations, how a mixture of 1.25 g of benzoic acid tertbutylbenzene can be separated by applying the separation of 2 components by liquid-liquid extraction.Suppose you want to determine the eutectic melting point of a eutectic mixture of adipic acid (literature MP 153 degree C) and salicylic acid (literature MP 158 degree C) .What would you do and what would expect to observe? Be sure to include a very specific detailed plan that any inexperienced organic chemistry lab student could follow if they were to use your procedure.We want to extract terpenoids from an aqueous sample by continuous liquid-liquid extraction. Which of the following solvents is not suitable for this purpose? Why? Propanone (acetone), dichloromethane, heptane.
- 1. An organic student did an experiment extracting benzoic acid from a mixture of other organic substances. Other analyses of the obtained sample confirmed the presence of benzoic acid. The student also measured the melting point of the white solid, 117.4-121.6 oC. The literature mp of benzoic acid is 122.3oC. What can you conclude about the sample? Select one. Group of answer choices The sample of benzoic acid contains soluble impurities. The student obtained a good yield of benzoic acid. The sample of benzoic acid contains insoluble impurities. The student obtained pure benzoic acid from the extraction. The student obtained a poor yield of benzoic acid. 2. Which phenomenon are sometimes confused with melting during mp analysis? Select all that apply. Group of answer choices decomposition cracking shaking sagging/shrinking sweating solidifying 3. Study the bond types in the compound shown. Select the type(s) of intramolecular force(s) you predict the substance to exhibit. Select all…A student is given a solid mixture containing 2 polar components and 1 nonpolar component. The student is asked to separate the nonpolar component by solid-liquid extraction. Which of the following solvents is the most appropriate to use for the extraction? Group of answer choices methanol (CH3OH) H2O hexane (C6H6) ethanol (CH3CH2OH)A bloodhound, with an acute sense of smell, sits at one end of a long, unventilated corridor.At the other end of the corridor a small amount of an aerosol is released containing the volatile, fragrant compounds: acetaldehyde (C2H4O) jasmine lactone (C10H16O2) acetoin (C4H8O2) hexyl acetate (C8H16O2) 1-octen-3-one (C8H14O) Rank the compounds in the chronological order they are detected by the hound. 1-octen-3-one acetoin jasmine lactone hexyl acetate acetaldehyde
