preview

6.03 Calorimetry Lab

Decent Essays

Question 1.

The boiling point elevation constant for water that was experimentally determined in this analysis was 0.4396 °C/m, which was derived from the slope of the trend line in Figure 2. This is slightly lower than the constant provided in lecture of 0.51 °C/m. This could be due to further evaporation of water from the solutions tested via refractive index after the boiling temperature was recorded.
Question 2. The freezing point depression constant for water that was experimentally determined in this analysis was 0.0479 °C/m, which was derived from the slope of the trend line in Figure 4. This is significantly lower than the constant stated in the literature of 1.86 °C/m.1 The freezing point temperature determined via cryoscopy should have been much lower in the high sucrose concentration solutions.
Question 3.
The method that was used as an attempt to determine the solubility limit of sucrose at room temperature consisted of creating a super-saturated solution by heating and dissolving excess sucrose. This solution was then allowed to come to room temperature over the course of a week with the hypothesis that the excess sucrose that was dissolved at elevated temperatures would crash out …show more content…

Also by using the molecular weight of glucose (342.3) it can be determined that the average degree of polymerization of the corn syrup solids is 2.669. These numbers were calculated based on boiling point data. A freezing point experiment was not conducted. This data makes sense, for corn syrup solids are created via hydrolysis of starch and consist of a mixture of glucose, maltose, and small glucose oligomers. The molecular weight/average degree of polymerization determined via this experiment directly correlates with that

Get Access