Copper in Silver Nitrate Lab

The experiment is to observe a variety of chemical reactions and to identify patterns in

Used stirring rods to completely remove copper from that wire. And then completed the removal of copper using 5 drops of 6M HCl, adding it onto copper. There will produced copper in a solution. Connected Buchner flask to the vacuum line and place filter paper in it to completely washed off the copper. Then, add 95% ethanol to copper and leave it for 1 min and turned section back for 5 mins. Measured mass of clean, dry watch glass. Transfer copper to watch glass and dry it under heat lamp for 20 mins, allowed it to cool to room temperature and then accurately determine its mass.

The purpose of the experiment is to cycle solid copper through a series of five reactions. At different stages of the cycle, copper was present in different forms. First reaction involves reaction between the copper and nitric acid, and copper changed from elemental state to an aqueous. The second reaction converted the aqueous Cu2+ into the solid copper (2) hydroxide. In the third reaction Cu(OH)2 decomposed into copper 2 oxide and water when heated. When solid CuO reacted with sulfuric acid, the copper returned to solution as an ion (Cu2+). The cycle of reactions was completed with the reaction where elemental copper was regenerated by Zn and Cu

5. Was there any evidence that some of the copper (II) chloride was left in the beaker? Explain.

2. Using the tweezers, lift the steel wool out of the vinegar and shake if gently over a paper towel.

21) After all of the solid dissolves, move the flask from the hot plate and allow it cool to room temperature. After a while, crystals should appear in the flask.

Then 8.0g of copper sulfate crystals were placed inside the beaker and the mass was recorded for the actual crystals. 50 mL of water was added to the beaker with the crystals. The ring stand was set up with the wire mesh on it and one partner should place the mixture in the beaker on it should be heated without letting the mixture boil. Stir the mixture and heat until the crystals are dissolved. While one partner does this, the other should obtain 1.5g of iron filings in a measuring cup and records the mass. Then the iron filings should be added small amounts at a time to the heated solution. Stir continuously until all the mixture is added to the beaker. Then it sat for 10 minutes and observations were recorded. Record the mass of a filter paper and set up a filtration apparatus with the filter paper in a funnel over an Erlenmeyer flask. Decant the liquid through the paper slowly trying not to allow any solid to get on the filter paper. Then with de-ionized water, rinse your solid in the beaker and let the solid settle then decant the liquid. Repeat the washing twice more and in the last time guide all the solid into the filter paper. Then place the filter paper on a watch glass and then into a warm oven to dry. After it is cool, record the mass of the watch glass, filter paper and solid. If there is not enough time to cool, you may have to do it the next

8. Repeat step 7 with H2SO4, except that you should use a 10 mL graduated cylinder of H2SO4 and adding 15 mL water.

XIV. Record your observations of the dried, cooled copper metal and weigh the recovered copper.

3) Repeat the drying process just to be sure that the copper is completely dry, and again determine the mass of the copper and the beaker.

Purpose: The purpose of this experiment was to observe the many physical and chemical properties of copper as it undergoes a series of chemical reactions. Throughout this process, one would also need to acknowledge that even though the law of conservation of matter/mass suggests that one should expect to recover the same amount of copper as one started with, inevitable sources of error alter the results and produce different outcomes. The possible sources of error that led to a gain or loss in copper are demonstrated in the calculation of percent yield (percent yield= (actual yield/theoretical yield) x 100.

The lab performed required the use of quantitative and analytical analysis along with limiting reagent analysis. The reaction of Copper (II) Sulfate, CuSO4, mass of 7.0015g with 2.0095g Fe or iron powder produced a solid precipitate of copper while the solution remained the blue color. Through this the appropriate reaction had to be determined out of the two possibilities. Through the use of a vacuum filtration system the mass of Cu was found to be 2.1726g which meant that through limiting reagent analysis Fe was determined to be the limiting reagent and the chemical reaction was determined to be as following:-

Weigh out the necessary grams of Copper Sulfate Pentahydrate. The 40-degree group weighed out 40 grams. (See Figure 1)

When the zinc was added to the copper (II) sulfate solution, the solution started to bubble. As the solution was stirred, it turned a cloudy blue. Small flecks of a brown solid were visible. As the solution became colorless, the brown solid settled to the bottom of the beaker. The solid formed was copper in its elemental state. The color faded from the solution as the copper ions slowly formed into solid copper. The copper was poured into a funnel with filter paper and washed three times with 25 mL

For the displacement reaction, an excess amount of zinc powder is added to the measured amount of aqueous copper (II) sulphate. The temperature change over a period of time has to be measured and thus, the enthalpy change for the reaction can be measured.