preview

Ethyl-2-Diphenylethene Lab Report

Satisfactory Essays

The purpose of this study was to conduct a bromination reaction to manufacture ethyl (2S,3R)-2,3-dibromo-3-phenylpropanoate from ethyl trans-cinnamate utilizing hydrogen bromide, hydrogen peroxide, and ethanol. However, due to an error in the mechanism, the reaction was performed under the same equivalent conditions with trans-diphenylethene to yield 1,2-dibromo-1,2-diphenylethane. Subsequently, a debromination reaction was performed to synthesize diphenylacetylene from the product, 1,2-dibromo-1,2-diphenylethane, utilizing potassium hydroxide and ethylene glycol. Both reactions were performed based on the principles of green chemistry: specifically increasing the atom economy, minimizing the syntheses of hazardous chemicals, utilizing safer solvents, preventing pollution and preventing accidents in the process.1 In order to evaluate the purity, each product was analyzed by obtaining the TLC and melting point range and running the samples in the Infrared spectrometer, Gas chromatography mass spectrometer, and Nuclear magnetic resonance spectrometer. Based on the mass of solid product obtained, the percent yield for ethyl (2S,3R)-2,3-dibromo-3-phenylpropanoate, 1,2-dibromo-1,2-diphenylethane and diphenylacetylene were calculated to be %, %, and % respectively.

Get Access