Marwah Alabbad Analysis and Identification of two Geometric Isomers post Lab 9/2/15 1) As conducted in pre lab question, melting point for Maleic acid is 139- 140◦C and Furmaic acid is 287◦C, and in the lab experiment the sample of A and B was identified first by test the melting point for each sample, and the result came as test tube B melted faster than test tube A, which leads to test tube A is Furamic acid and test tube B is Maleic acid, because of the low melting point for Maleic acid, it
Stereochemistry Post Lab Report Reference: Experimental Organic Chemistry: A Miniscale and Microscale Approach, 6th ed., by Gilbert and Martin, Chapter 7 Discussion: The main purpose of this experiment was to study the mechanism of the isomerization of dimethyl maleate to dimethyl fumarate as well as to explore the different properties of enantiomers using (R) and (S) Carvone oils, such as polarimetry and odor. A percent yield was calculated based upon the original amount of dimethyl maleate added
RADICAL HALOGENATION AND GAS CHROMATOGRAPHY Abstract In radical halogenations lab 1-chlorobutane and 5% sodium hypochlorite solution was mixed in a vial and put through tests to give a product that can then be analyzed using gas chromatography. This experiment was performed to show how a radical hydrogenation reaction works with alkanes. Four isomers were attained and then relative reactivity rate was calculated. 1,1-dichlorobutane had 2.5% per Hydrogen; 1,2-dichlorobutane had 10%; 1,3-dichlorobutane
Name: Chen Yao Le Lab Group: Tues Email: A0111185@nus.edu.sg Matriculation Number: A0111185R Date of Experiment: 17 February 2015 Experiment 6: Synthesis, Electronic Spectra, Structural Isomerism: Octahedral Co(III) complexes with Chloride and Ethylenediamine Ligands Abstract: In this experiment, Δ/Λ-[Co(en)3]Cl3∙4H2O was synthesized and the absorbance in UV-vis spectrum was recorded
Moldovan Submitted: Nov. 22nd, 2010 By: Jackie Minnick (Partners Amanda Verwoerd & Kersti Ojamaa) Study of stereospecificity in mushroom tyrosinase and the inhibiting effects of thiourea, cinnamic acid and benzoic acid. Jackie Minnick This paper reports experiments on the stereospecificity observed in the monophenolase and diphenolase activities of mushroom tyrosinase and the inhibiting effects of thiourea, cinnamic acid and benzoic acid. The enantiomer L-DOPA and D-DOPA were assayed. The Vmax and
Valbenazine, an analog to Tetrabenazine, is an emerging approach to the treatment of TD that is showing potential. Valbenazine is considered a purified parent drug of the positive alpha isomer of Tetrabenazine. One advantage of this emerging drug is the less adverse side effect profile, and the once-a-day administration, as compared to Tetrabenazine, which has a more adverse side effect profile and requires frequent intake due to its rapid metabolism (Muller, 2015). Approval hurdles for Valbenazine
Sulphonation – The Process Most electrophilic substitution reactions are irreversible but sulfonation is an exception. Treatment of benzene with "oleum" (a solution of SO3 in concentrated sulfuric acid) will give the sulfonic acid, the electrophilic species being sulfur trioxide which is Lewis acidic. Fig – 1 Sulphonation : Benzene equation The sulfonic acid can be converted back by treatment with hot aqueous acid. The reason for this reversibility is the fact that the Wheland intermediate is overall
this experiment, identification of the unknown ketone is accomplished through thin layer chromatography, melting point, and 1H-NMR spectroscopy. The unknown ketone is from a homologous series of methyl ketones. CH3CO (CH2) nCH3 The first step in the lab is the preparation of the solvent used in the developing chamber for thin
eCTD/CTD/ACTD Implementation in Southeast Asia Harv Martens ICH M2 JPMA Extedo, Inc. The views and opinions expressed in the following PowerPoint slides are those of the individual presenter and should not be attributed to Drug Information Association, Inc. (“DIA”), its directors, officers, employees, volunteers, members, chapters, councils, Special Interest Area Communities or affiliates, or any organization with which the presenter is employed or affiliated. These PowerPoint slides are the
Executive Summary On December 3, 1984, toxic poisonous methyl isocyanate gas leaked from Union Carbide India Limited (UCIL 's) pesticide plant in Bhopal. The gas leak triggered a disaster that is now widely recognized as the world worst industrial catastrophe. Thousands of people were killed instantly and more than 25,000 people have died of gas-related illnesses, several thousands more maimed for life since. Union Carbide negotiated a settlement with the Indian Government in 1989 for $470 million