EXPERIMENTAL Part A of this experiment was essential because it set up the chemical solutions needed for Part B and C, as well as the equipment that was used throughout the entire experiment. To start, a 300mL solution of 2M HCl was prepared with the stock solution of 6M HCl. For this, 200mL of deionized water was collected and added it to a 400mL beaker. Then, 100mL of 6M HCl was added to the water. Next, 150mL of 2M NaOH was prepped by 50mL deionized water combined with 100mL 3M NaOH in another 400mL beaker. Before the experiment began, the LabQuest was plugged in and turned on. The temperature probe was then plugged into channel one of the LabQuest. In order to fully set up the LabQuest, the interval was changed to 15 s/sample. Part B was responsible for the reaction of hydrochloric acid and ammonium hydroxide. The first of three sub-reactions were monitored when 2 Styrofoam cups were stacked together and placed in a 400mL beaker. The cups were filled with 50mL 2M HCl first while the initial temperature was recorded. After 3 or 4 readings, 2M NaOH was added in one smooth motion and stirred until the temperature reached a maximum or began to decrease. Once the data was collected, the mixture was disposed of and the equipment was rinsed and dried. Next, using the same method, the calorimeter was set up with 50mL 2M NaOH. After inserting the temperature probe and receiving 3 or 4 readings, 50mL 2M NH4Cl was poured in and the cup was stirred until the temperature reached a
For part B, 50 mL of an assigned 50 mL pH solution of either 1 M HCl, 1 M NaOH, lemon juice, and 50 mL of household bleach all in separate 250 mL beakers are to be used. For part C, a hot plate or ice are to be used to make the 1.0 mL assigned temperature specific water. This experiment will also use the 1.0 mL of 0.1 Phosphate buffer.
13. The temperature of the water was measured prior to the tube being placed in it and the temperature of the Hydrochloric Acid was measured after it 's temperature had adjusted.
The control experiment for this investigation will be the experimental setup of 5 trials using 5oC as the temperature. All the steps in the method will be followed.
Experiment 2 focused on finding the enthalpy of solution of magnesium chloride. Testing the enthalpy of solution started with measuring out 10 mL of deionized water in a graduated cylinder for three separate trials, each trial having a different mass of magnesium chloride. The water was then poured into a well of a Styrofoam calorimeter then the initial temperature of water was taken using a temperature probe and the LoggerPro programming. A measured amount of magnesium chloride was placed in the same well as the water in the calorimeter,
After the twenty minutes elapsed, the flask was cooled to room temperature and then titrated with the remaining NaOH until the colorless solution remained pink. The final volume was then recorded. While solution #1 was heating the same process was repeated with solution#2 and the second burette
The next step in this lab is to rinse the Erlenmeyer flask with distilled water down the drain and then repeat the experiment, this time adding 10 ml of 0.10M KI and 10 ml of distilled water to the flask instead. The flask should again be swirling to allow the solution to succumb to the same temperature as the water bath and once it has reached the same temperature, 10 ml of 3% H2O2 must then be added and a stopper must be immediately placed on the flask and recording should then begin for experiment two. After recording the times, the Erlenmeyer flask must then be rinsed again with distilled water down the drain. After rinsing the flask, the last part of the lab can now be performed. Experiment three is performed the same way, but instead, 20 ml of 0.10 ml M KI and 5 ml of distilled water will be added and after the swirling of the flask, 5 ml of 3% H2O2 will be added. After the times have been recorded, data collection should now be complete.
The room temperature was measured throughout the lab and kept constant at 24°C (+/- 1°C), as the lab was conducted during the same time of
4. Remelt the contents of the tube and add the counterpart component based on the given schedule. Ask the demonstrator to adjust the cooling water between mixtures. During the experiment, record and plot the data obtained for all mixtures listed. The experiments are stopped as follows:
The start of the experiment consisted of filling up four beakers with de-ionized water to 150 ml. After the beakers were filled to the appropriate amounts they were then labeled with the
The four salts that were given were ammonium chloride (NH4Cl), ammonium nitrate (NH4NO3), sodium thiosulfate (Na2S2O3), and magnesium sulfate (MgSO4). With the intention of saving time, my group was given only ammonium chloride and ammonium nitrate to do and then we would compare the results with the entire class. First, the probe needed to be calibrated and in order to do that three 250 mL beakers were filled to 50.0 mL of distilled water. One beaker was room temperature and a thermometer was placed in it that measured to 19.9 degrees Celsius. Another beaker was cold water (iced added to it) and a
This experiment was performed to determine the heat of neutralization between Hydrogen chloride (HCl) and Sodium hydroxide (NaOH). A temperature probe was used to measure the temperature of the reaction when the base (NaOH) was poured into the acid (HCl). The data was collected on logged on LoggerPro.
Step 1 and 2 was repeated by using distilled water by replacing the test solution.
Equipment, Materials, and Method The equipment used were a jacketed batch reactor beaker, cooling water circulation system, computer, LabPro temperature probe and conductivity probe, mixing stand and magnetic stir bar. The materials used for this reaction were a 0.08M NaOH solution and a 0.1M ethyl acetate solution. A 20% excess Ethyl acetate was used to ensure NaOH was the limiting reactant.[1] NaOH was chosen for the limiting reactant because of its high conductivity relative to Ethyl acetate. The extent of the reaction was monitored by measuring the conductivity throughout the reaction. With NaOH being the limiting reactant, the change in conductivity is more visible, and the termination of the reaction can
Purpose: You will determine the molar heat of neutralization of 1.00 M HCL and 1.00 M NaOH in Kilojoules.
In this experiment, 25mL of HCl will be mixed with 25mL of NaOH in a calorimeter. The temperature change of the solution will be measured and used to determine the heat released by the solution according to the formula q=mCspT. The mass of the solution will then be used to determine