3.1.2 Formation of NiOOH onto SPNE Ni pastes of SPNE were electrodeposited by CV to form Ni(OH)2 and NiOOH as the sources of Ni(II) and Ni(III) ions, respectively, onto the SPNE for 30 cycles from 0 to 1.5 V in 0.1 M NaOH. In the first scan, redox couple peaks of SPNE appeared at 0.614 V. The redox couple peaks of Ni(II)/Ni(III) onto SPNE appeared at 0.538 V (Figure 1(a)). This result shows that Ni(II)/Ni(III) formed well. Moreover, the electrochemical reactions of Ni(II)/Ni(III) redox couples have been reported as follows:[28] Ni + 2OH- → Ni(OH)2 + 2e- Ni(OH)2 + OH- → NiOOH + H2O + e- The CV of the electrodeposited SPNE in 0.1 M NaOH showed one pair of quasi-reversible redox peaks at E1/2 = 0.538 V vs. Ag/AgCl, as shown in Figure 1 (b). The current density on the SPNE is also shown in the inset of Figure 1(b) as a function of the scan rates. The inset in Figure 1(b) shows that the anodic peaks [(Ip)a](r = 0.99462) and the cathodic peaks [(Ip)c](r = 0.99475) of the Ni(OH)2/NiOOH-SPNE electrode increased linearly with the square root of the scan rate (v1/2) in the range of 0.01 to 0.2 V/sec. These results suggest that Ni(II)/Ni(III) in the SPNE is a fast and reversible redox material to investigate the glucose level [29]. 3.1.3 Morphology of SPNE The morphology of SPNE was observed by scanning electron microscopy (SEM). The typical FE-SEM images of the pristine carbon printed ITO electrode and 50 wt% SPNE electrode are shown in Figures 2(a) and 2(b), respectively.
In Part 1 of the lab, a solar cell was created and tested for its capability to conduct electricity. After researching the processes that contribute to the conductive property, it was found that the oxidized substance is the dye, as it donates an excited electron to the titanium oxide. Consequently, titanium oxide is reduced before it donates an electron to the cathode. The electrolyte solution was found to replenish the dye with electrons so it could continue to act as a reducing agent.
The United States prides itself on being a democracy in which equal opportunity and the pursuit of happiness are guaranteed rights for all citizens. There is no uncertainty in the loyalty that Americans have towards this promise of natural, unalienable rights. However, as Michael Foucault explains in Discipline and Punish, the power structures present in society infringe on our rights to equal opportunity and happiness by forcing us to abide by social norms and expectations. Using Barbara Ehrenreich’s experience as a low-wage worker in Nickel and Dimed as an example, it is clear that the power structure of observation that Foucault describes disciplines low-wage workers to behave and live in a way society deems appropriate.
The performance of the electrode depends on two important factors namely microstructure and morphology and the effect of doping. These two factors influence the type of cathode materials that can be chosen for the battery. Intercalation and deintercalation happen along particular crystallographic planes and headings, so higher crystallinity enhances terminal
1. Purpose: to clarify the mechanism for the cycloaddition reaction between benzonitrile oxide and an alkene, and to test the regiochemistry of the reaction between benzonitrile oxide and styrene.
Received a call from Beth. Her computer lost its trust relationship to the domain after upgrading to Windows 10. Removed the computer from the domain. Attempted to join the computer to the domain but it failed. I kept receiving an error saying the server could not be found after entering the domain credentials. Ran an ipconfig /all and found she wasn’t getting the servers IP for DNS. Logged into their Linksys router and found the server was listed in the DNS. Added the Servers IP address. Reboot her computer and confirmed I was able to join the domain.
The diagram below shows a labelled circuit which is used for the experiment. This is set up by collecting all equipment needed and attaching the DC power supply to the ammeter with a wire this is all connected to the anode and cathode with a red and black wire to differentiate between the two electrodes. The two electrodes are shown to be placed in a beaker of copper sulphate
Referring back to the statistics on password length in section 3.1.5 for rockyou.com, attacker one would be able to crack all passwords less than eight characters being 33.00% of users in little over an hour. Since 26.00% of the users from the website used only lower alpha passwords and 2.76% used only mixed alphanumeric passwords, the results differ tremendously if attacker one only covered this character set on the 28.76% of users.
/**-------------------------------------------------------- 1. Name: JokeClientAdmin.java 2. Java version used build 1.5 3. Precise command-line compilation examples / instructions: > javac JokeClientAdmin.java 4.
All the data was fitted satisfactorily using the equivalent circuit shown in Fig. 7. Where, Rs, CPE1 and R1 represent solution resistance, a constant- phase element corresponding to the double layer capacitance and the charge transfer resistance, respectively. CPE2 and R2 were added to account for the electrical elements of the outer layer. The following formula expressed the electrode impedance, Z, as follow:
Connected into J’s computer because she was having issues with her VMWare, she also stated her mouse started moving on its own. Checked for any remote software on her computer besides our own. Updated Java and removed all old version. Installed all windows updates and reboot her computer. She was able to connect to her VMWare, but it would close shortly after. Ran a repair and VMWare. Rebooted her computer, and confirmed she was able to access her
A Mohr pipette allowed for the accurate measuring of a standard solution, by recording the final and initial pipette readings of 0.200 M Fe(NO3)3 and 0.00200 M KSCN. With Le Chatlier’s principle in mind, an excess of 0.200 M Fe(NO3)3 was used rather than 0.00200 M as a flooding technique to keep Fe(NO3)3 constant throughout the reaction and favor the products. To determine the equilibrium solutions, four 50 ml beakers were obtained by recording their final, initial, and total volume dispensed. Beaker 1 consisted of 5 ml Fe(NO3)3, 2 ml KSCN, and 3 ml H2O. Beaker 2 contained 5 ml Fe(NO3)3, 3 ml KSCN, and 2 ml H2O. Beaker 3 consisted of 5 ml Fe(NO3)3, 4 ml KSCN, and l ml H2O. Lastly, beaker 4 contained 5 ml Fe(NO3)3 and 5 ml KSCN. Next, the absorbance values were calculated by placing each solution into a 470 nm colorimeter, then using Logger Pro to determine the absorbance for each solution when given the concentration values. As seen in table 3, the absorbance value for the standard solution was 0.818 with a [Fe(SCN)2+] concentration of 2.00 10-4 M. To reduce error, Mohr pipette readings were recorded to two decimal places and data was not recorded on the meniscus of the line. This allowed for a higher quality of recordings and the avoidance of biased
As a hash can be generated by anyone and attach to a message, the intruder can modify the original message and recalculate the hash and append to it. This change can’t be detected at the receiving end as there is no chance of knowing the message or the hash.
In order to let Syringe inject the target process, we create a remote thread in the process, and then the thread loads Serum into itself. Because of the Windows design, we cannot control an existing thread of a process, but we can create a thread in a certain process to do a specific task. We use CreateRemoteThread() [30] to create a thread in the certain process we want to hook. The thread calls the LoadLibraryA() [31] function that loads Serum, so that the process does whatever we want it to do in Serum.
For this lab, lead (II) nitrate (Pb(NO3)2) and potassium chromate (K2CrO4) will be reacted together to demonstrate double replacement reaction between 2 ionic compounds. This was shown when chromate replaced the nitrate and formed lead (II) chromate, and when the nitrate replaced the chromate and formed potassium nitrate, which is shown in the
slope for January is ((12 - 10) / (31 - 1) = 2/30 = 1/15