.A sample of alfalfa meal weighing 2.0 g is analyzed by Kjeldahl method for the percentage of nitrogen. The liberated NH3 is caught in a solution of H3B03, and 8.23 ml of HCI are required in the subsequent titration. A sample of pure (NH4)2SO4 (132.12) weighing 0.61 g is treated with excess NaOH and the liberated NH3 (17.04) is also caught in H3BO3. The resulting solution requires 20 ml of the acid for titration. Calculate the percentage of protein in the sample using 6.25 as the factor.

Fundamentals Of Analytical Chemistry
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ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter20: Applications Of Oxidation/reduction Titrations
Section: Chapter Questions
Problem 20.25QAP
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.A sample of alfalfa meal weighing 2.0 g is
analyzed by Kjeldahl method for the
percentage of nitrogen. The liberated NH3 is
caught in a solution of H3BO3, and 8.23 ml of
HCl are required in the subsequent titration. A
sample of pure (NH4)2SO4 (132.12) weighing
0.61 g is treated with excess NaOH and the
liberated NH3 (17.04) is also caught in
H3BO3. The resulting solution requires 20 ml
of the acid for titration. Calculate the
percentage of protein in the sample using
6.25 as the factor.
Transcribed Image Text:.A sample of alfalfa meal weighing 2.0 g is analyzed by Kjeldahl method for the percentage of nitrogen. The liberated NH3 is caught in a solution of H3BO3, and 8.23 ml of HCl are required in the subsequent titration. A sample of pure (NH4)2SO4 (132.12) weighing 0.61 g is treated with excess NaOH and the liberated NH3 (17.04) is also caught in H3BO3. The resulting solution requires 20 ml of the acid for titration. Calculate the percentage of protein in the sample using 6.25 as the factor.
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