0.2 gm of ethanol was acetylated with acetic anhydride in presence of pyridine (1:3), neutralization of the resulted solution required 20 ml of 0.1 N NaOH, while the blank titration reqiuered 40ml of NaOH. Calculate the percentage of hydroxyl group in this sample ?
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- how to analyse alkaloids using Acid dye colorimetry method and HPLC method? Discuss atleast 5 sentences eachE. TESTS FOR PHENOLIC COMPOUNDSPhenolic compounds such as phenol, salicylic acid, etc., give characteristiccolors with FeCl3 and Millon’s Reagent.1. Ferric Chloride TestAdd 5 drops of FeCl3 solution to 4 different test tubes containing 1 mL each ofdilute solutions of the following compounds and note the color obtained.a. Phenol _______________________________________________________________b. Salicyclic acid ___________________________________________________________c. Resorcinol _______________________________________________________________d. Picric acid _______________________________________________________________2. Millon’s TestPrepare another set of 4 test tubes containing 1 mL each of the solutions listedbelow. Add 3 drops of Millon’s reagent to each and place all the test tubes in aboiling water bath. Note the color formed.a. Phenol _______________________________________________________________b. Salicylic acid ___________________________________________________________c.…SHOW COMPLETE SOLUTIONS Q3. Which isolate has A260/280 ratio of above 2.0?
- 3.0cm³ of redistilled sebacoyl chloride was obtained (density =1.12gcm-3).And dissolved in 50cm³ of dry dichloromethame . 2.2g of diaminohexane was dissolved in 25cm³ of water . 1. Calculate the molar ragione of diamine to acid chloride used 2 .This time using 1.6g of diaminohexane ,calculate the new molar ratioA mixture containing compounds A and B in methylene chloride (CH2Cl2) was extracted in a separatory funnel containing aqueous HCl. Which compound migrates to the aqueous layer? Why?5. 1. What is the purpose of testing distilled water and laboratory ethanol in the testing of ethanol? 2. During the experiment, you recorded the vapor temperature of the samples. Does the literature B.P. of ethanol correspond to the recorded temperatures? Why or why not? 3. Based on the iodoform test, did your distillate portion contain ethanol and/or water? Explain?
- A solution of the following three compounds in ether is extracted first with aqueous HCl, secondly with aqueous NaHCO3. Where will each of the three compounds reside after the procedure: the NaHCO3 extract, the HCl extract, or the ether layer? Please explain with the help of pKa numbers. (image of compounds attached)A mixture is made up of low molecular weight carboxylic acid, alcohol and ester. What one step procedure can you use to extract the ester component from the mixture? Describe the process brieflyDefine Separation of benzoic acid and cyclohexanol by an extractionprocedure ?
- 8.For end-group analysis, 0.8632 g of a carboxyl terminated polybutadiene (CTPB) sample dissolved in 1:3 mixture of ethanol and toluene consumed 5.2 ml of 0.1240 N alcoholic potassium hydroxide solution in titration using phenolphthalein as the indicator. Calculate the molar mass of the polymer.A Student added 1.5 ml of 3 M Methyl Magnesium Bromide to a conical vial containing Benzophenone & diethyl ether, after 30 minutes he added dilute sulfuric acid and isolated the product. Identify the Major product. a) b) c) d)What is the predominant form of cyclohexylamine at pH 9.5? Approximately what fraction is in this form?