1. Calculate the percent of SiO, in the mixture by using the equation: %= part * 100 whole 2. Calculate the percent of NaCl in the in the mixture. (continued on back!) Fundamental Chemistry I 44 3. Calculate the percent recovery for the experiment.
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- The method of standard additions was used to determine nitrite in a soil sample. A 1.00-mL portions of the soil extract sample was transferred to four 25-mL volumetric flasks. To each flask, increment volumes of a 1.00 x10-3M nitrite was added according to the table below. A colorimetric reagent was added to each flask to convert the nitrite into a colored product, and finally diluted to volume. What is the concentration of the nitrite in the soil extract based on the absorbance data below (with blank correction included)? Vol. of standard nitrite added, ml Absorbance 5.00 0.079 10.00 0.161 15.00 0.236 20.00 0.318 25.00 0.403using exactly 5.00 mL of 0.0400 M stock CuSO4 solution. Add 100 mL of water. Data for Part IMass of empty dish: 32.470 g empty dishVolume of 0.0400 M solution: 5.00 mL CuSO4 solution.Mass of dish and 0.0400 M solution: 37.497 g dish and solutionMass of dish and CuSO4 solid: 32.503 g dish and CuSO4 solidCalculations for Part I1. Calculate the mass of solution2. Calculate the mass of solid CuSO4 dissolved in the solution.3. Calculate the number of moles of solid CuSO4 dissolved in the solution.4. Calculate the mass of water evaporated from the solution.5. Calculate the density of solution, (g solution/mL solution).6. Calculate the % by mass, CuSO4 in solution (100 x g CuSO4/g solution).7. Calculate the molality of solution (moles CuSO4/kg solvent).8. Calculate the molarity of solution (moles CuSO4/L solution).9. Given that the true molarity is 0.0400 M, calculate the percent error of your result.using exactly 5.00 mL of 0.0400 M stock CuSO4 solution. Add 100 mL of water. Data for Part IMass of empty dish: 32.470 g empty dishVolume of 0.0400 M solution: 5.00 mL CuSO4 solution.Mass of dish and 0.0400 M solution: 37.497 g dish and solutionMass of dish and CuSO4 solid: 32.503 g dish and CuSO4 solidCalculations for Part I1. Calculate the mass of solution? 5.027 g 2. Calculate the mass of solid CuSO4 dissolved in the solution? 0.033 g 3. Calculate the number of moles of solid CuSO4 dissolved in the solution? 2.07 x 10-4 mol4. Calculate the mass of water evaporated from the solution? 0.0414 M5. Calculate the density of solution, (g solution/mL solution)?6. Calculate the % by mass, CuSO4 in solution (100 x g CuSO4/g solution)?7. Calculate the molality of solution (moles CuSO4/kg solvent)?8. Calculate the molarity of solution (moles CuSO4/L solution)?9. Given that the true molarity is 0.0400 M, calculate the percent error…
- Which sentence is false about gravimetric analysis? a. It is used for inorganic b. It is used to assay barium c. It is used to assay of d. Relative precision 3% to 4%mass of dish 1631.5 g mass of dish and mix 1822 g mass of dish and agg. after extraction 1791g mass of clean filter 25 g mass of filter after extraction 30 g mass of agg. in 150 ml solvent 1.2g if Ac% 5% find the volume of the solventGrain sample was found to contain 6.6% moisture. A 5.3000 g as received sample was placed ina crucible (29.5033g tare) . The ashed crucible weighed 30.0055 g.Calculate % ash on a) as received basis b) dry basis
- A new method is proposed to simultaneously detectand separatefour foodadditives by reversed-phase liquid chromatography. The data were obtained using theliquid chromatographic column with a flow rate of 0.5 mL per min and with the followingparameters: Pore size 100 A Particle Size 3.5 Internal diameter 4.6 mm Length 150 mm The food additives found in the sample resulted in the following data: ( see image for table) a.Calculate the number of plates from each peak. b.Calculate the plate height for the column. c.Retention factor for each peak.Standardization of EDTA Solution Weight of pure CaCO3: 0.2517 g % Purity of CaCO3: 98.0% Total volume of standard CaCO3 solution: 250.00 mL Trial 1 2 3 Volume of standard CaCO3 solution (ml) 25.00 25.00 25.00 Final Volume Reading EDTA (ml) 24.30 47.95 24.72 Initial Volume Reading EDTA (ml) 0.00 24.30 0.20 Volume of titrant, EDTA (ml) Molarity of EDTA (M)ASSAY Calibration solutions Calibration solutions of naproxen in the range 5 – 25 μg/mL were prepared. Sample preparation 20 tablets weighing 12.3819 g were crushed to a fine powder. A portion of the powder (145.4 mg) was shaken with approximately 150 mL of acetic acid (0.05 M) for 5 min and then made up to volume in a 250 mL volumetric flask (stock solution). Approximately 50 mL of the stock solution was filtered and a 25 mL aliquot was diluted to 100 mL in a volumetric flask. 10 mL of the resulting solution was further diluted to 100 mL with acetic acid (0.05 M). Analysis The standards and sample solutions were analyzed by HPLC under the following conditions: Column: octadecylsilyl (ODS), 4.6 mmx150 mm, mobile phase: acetonitrile : 0.05 M acetic acid (85:15), flow rate: 1 ml/min, UV detection at 243 nm. Results: A calibration curve of concentration versus peak area was constructed for the standard solutions and gave the straight-line equation: y = 3555.6x + 85, r = 0.9999 The area…
- Stock iron(II) solution (200Ug mL-1 Fe) ferrous ammonium sulfate hexahydrate mass= 0.1437g, transfer it to a 100 ml beaker. add 15 ml approx of water and 15m1 'approx of dilute sulphuric acid (2M H2SO.). then transfer FeII to 100 ml flask makeup to the mark with water. calculate the moles of ferrous ammonium sulfate hexahydrate solution in unit ug/mL.Standardization of Sodium Thiosulfate Solution Primary Standard used: Potassium Dichromate Formula mass of 1o standard: __________________ % Purity of 1o standard: 99.80% Trials 1 2 3 Weight of K2Cr2O7 (g)Weight of K2Cr2O7 (g) 0.0315 0.0331 0.0380 Final Volume Reading Na2S2O3 (ml) 27.50 27.50 34.90 Initial Volume Reading Na2S2O3 (ml) 1.10 0.00 1.00 Net Volume Na2S2O3 used (ml) Molarity of Na2S2O3I got a task in analytical chemistry to calibrate, standardize, verify and validate an analytical balances