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- why would you write 13.90 when only two sig figs were given? Where does the extra "precision" come from?Quality assurance. Tin can be leached (dissolved) into canned foods from the tin-plated steel can. (a) For analysis by inductively coupled plasma–atomic emission, food is digested by microwave heating in a Teflon bomb (Figure 2-18) in three steps with HNO3, H2O2, and HCl. CsCl is added to the final solution at a concentration of 1 g/L. What is the purpose of the CsCl?A certain mixture of gasoline obtained from a petroleum refinery plant was found to contain only isooctane (C8H18; FM = 114.22), methyl tert-butyl ether (C5H12O; FM = 88.15), and tetraethyl lead (C8H20Pb; FM = 323.4), a gasoline preservative. Upon complete combustion of 0.4582 g sample, it was found out that the mass of the CO2 (FM = 44.01) absorbent increases by 1.0702 g, while the mass of residue PbO (FM = 223.2) was determined to be 0.0964 g. From this data, calculate the following: a. % (w/w) C8H18b. % (w/w) C5H12Oc. % (w/w) C8H20Pbd. % (w/w) Pb (FM = 207.2) Answer a to c only
- A certain mixture of gasoline obtained from a petroleum refinery plant was found to contain only isooctane (C8H18; FM = 114.22), methyl tert-butyl ether (C5H12O; FM = 88.15), and tetraethyl lead (C8H20Pb; FM = 323.4), a gasoline preservative. Upon complete combustion of 0.4582 g sample, it was found out that the mass of the CO2 (FM = 44.01) absorbent increases by 1.0702 g, while the mass of residue PbO (FM = 223.2) was determined to be 0.0964 g. From this data, calculate the following: a. % (w/w) C8H18b. % (w/w) C5H12Oc. % (w/w) C8H20Pbd. % (w/w) Pb (FM = 207.2) Answer Letter D onlyA certain mixture of gasoline obtained from a petroleum refinery plant was found to contain only isooctane (C8H18; FM=114.22), methyl tert-butyl ether (C5H12O); FM=88.15), and tetraethyl lead (C8H20Pb; FM=323.4), a gasoline preservative. Upon complete combustion of 0.4582 g sample, it was found out that the mass of the CO2 (FM = 44.01) absorbent increases by 1.0702 g, while the mass of residue PbO (FM = 223.2) was determined to be 0.0964 g. From this data, calculate the following: a. % (w/w) C8H18b. % (w/w) C5H12Oc. % (w/w) C8H20PbThe measurement of Li in brine (salt water) is used by geochemists to help determine the origin of this fluid in oil fields. Flame atomic absorption of Li is subject to interference by other elements. Atomic absorption of analysis of replicate sample of Li in a brine sample gave results in the table. a. Suggest a reason for the increasing apparent concentration of Li from sample 1 to 2. b. Suggest a reason for the increasing apparent concentration of Li from sample 1 to 3 c. Why do samples 4-6 give a nearly constant result? (What type of interference you think is being eliminated?
- To quantify the Cadmium content in a water sample, 5 aliquots of 10 mL were taken, adding to each one of them a volume of a standard solution of Cd (2 mg / mL); after the addition the final volume for all solutions was 50 mL. The absorbance reading was taken in an Atomic Absorption spectrophotometer, the data recorded were: Aliquot 1 2 3 4 5 Cd solution (mL) 0 1 2 3 4 Absorbance 0.163 0.240 0.319 0.402 0.478 Calculate the ppm of Cd.(Standard addition) Tooth enamel consists mainly of the mineral calcium hydroxyapatite, Ca10(PO4)6(OH)2. Trace elements in teeth of archeological specimen provide anthropologists with clues about diet and diseases of ancient people. Student at Dankook University measured the trace element strontium (Sr) in enamel from extracted wisdom teeth by atomic absorption spectroscopy. Solutions were prepared with a constant total volume of 10 mL containing 0.750 mg dissolved tooth enamel plus variable concentrations of added standard Sr. Added Standard Sr (ng/mL=ppb) 0 2.50 5.00 7.50 10.00 Emission Signal 28.0 34.3 42.8 51.5 58.6 (a) Make a graph showing the experimental data and the calculated straight line. (b) Find the concentration of Sr in the tooth ennamel in parts per million = μg/mL.Quinine in a 1.553-g antimalarial tablet was dissolved in sufficient 0.10 M HCl to give 250 mL of solution.A 10.00-mL aliquot was then diluted to 50.00 mL with the acid. The fluorescence intensity for the dilutedsample at 347.5 nm provided a reading of 196 on an arbitrary scale. A standard 100-ppm quinine solutionregistered 125 when measured under conditions identical to those for the diluted sample. Calculate the massin milligrams of quinine in the tablet.
- A) Find [B] = ,[E] = ,[T] =,[P] = , Does the incineration of the mixture meet regulatory requirements? B)Determine the emission rate (lb/hr) of HCl (MW= 36.45 g/mol) resulting from the incineration of 760 lb/hr of tetrachlorophenol (C6HOHCl4, MW = 231.9 g/mol C)Determine the DRE of HCl (MW= 36.45 g/mol) resulting from the incineration of 760 lb/hr of tetrachlorophenol (C6HOHCl4, MW = 231.9 g/mol). The outlet emission rate of HCl is given in the table in the textbook for question 12-2 as 4.3 lb/hr. The DRE is most nearly .. D)Calculate the concentration (grains/dscf) of particulates in the flue gas if the stack flow rate is 37,500 dscfm, oxygen in the flue gas is 7%, and the particulate emission rate is 20.3 lb/hr. Specify your numerical result to three decimal places, such as x.xxx. Do not include the units in the answer.1. An unknown sample of Cu2+ gave an absorbance of 0.262 in an atomic absorption analysis. Then 1.00 mL of solution containing 100.0 ppm Cu2+ was mixed with 95.0 mL of unknown, and the mixture was diluted to 100.0 mL in a volumetric flask. The absorbance of the new solution was 0.500. a) Denoting the initial unknown concentration as [Cu2+]i, write an expression for the final concentration [Cu2+]f, after dilution. Units of concentration are ppm. b) In a similar manner, write the final concentration of added standard Cu2+ designated as [S]f. c.) Find the [Cu2+]I in the unknownA spectrophotometric method for the quantitative analysis of Pb2+ in blood has a normal calibration curve for which Sstd=(0.296 ppb−1)×Cstd+0.003. What is the concentration of Pb2+ in a sample of blood if Ssamp is 0.397?