3. Why is it unwise to allow the solution of the Grignard reagent to remain exposed to air for an unnecessary period of time even if it is protected from moisture by the drying tube?
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- Can you list the possible sources of error that can affect the yield of a Grignard reaction followed by extractions?What indication in the "test tube test" (procedural step 9) will be given if Na3PO4 is the limiting reagent? What if BaCl2 is the limiting reagent? Explain whyWhy is it necessary to keep all materials dry in Grignard reactions?
- How should you choose a developing solvent when there is no specified reagent?On a separate (stapled) paper, outline a separation scheme for isolating benzoic acid from the reaction mixture. (similar to the one in Technique 2, Figure 2.1, Pavia).Why is it possible to use solvent-grade diethyl ether in the work-up procedure, whereas the more expensive anhydrous form must be used to prepare the Grignard reagent?
- Write the reaction involved in Ferrox Test. a. What is the species responsible? b. Why is phenol negative in Ferrox Test? Based on the theoretical result, what is the order of reactivity of primary, secondary, and tertiary alcohols in the Lucas Test? a. Lucas Reagent contains ZnCl2 in HCl. What is the role of ZnCl2?What is the chemical composition of the nitrating mixture? Why does the incoming nitro group go para and not ortho?Why does a 70:30 hexane:acetone mixture produce a more effective separation of pigments in spinach compared to a 50:50 hexane:acetone mixture? Explain thoroughly
- Compound X gives good recrystalisation results using the following three solvents ethanol,methanol,and dichloromethane .Which solvent will you select as the best solvent out of those three and why?Q1: Give one lysis buffer that is commonly used for western blotting experiments and include its components Q3: To make sure that you used a similar amount of samples, what important step should be done before proceeding the electrophoresis stage? Q4. Why is it necessary to store the prepared lysates in a very low temperature?Why is the 4-methoxyphenyl acetate organic layer subjected to washes with saturated sodium bicarbonate solution, water and brine when carrying out a separatory funnel extraction?