4. The %Mn in steel can also be determined spectrophotometrically by oxidizing the manganese to the intensely colored permanganate, MnO4. Standard solutions of permanganate gave the following absorbances (in a 1 cm cell): ABSORBANCE CONC. OF MnO4 (g/mL) 0.210 1.05 x 10-5 0.315 1.61 x 10-5 0.429 2.21 x 10-5 0.599 2.98 x 10-5 0.801 4.04 x 10-5 The following samples of steel were thoroughly reacted to convert the manganese ir permanganate and then diluted to 500.00 mL. WT. OF STEEL (g) ABSORBANCE 0.5886 0.611 0.3498 0.359 0.4555 0.482 Again using Excel, plot the calibration data and calculate the %Mn in the steel.
4. The %Mn in steel can also be determined spectrophotometrically by oxidizing the manganese to the intensely colored permanganate, MnO4. Standard solutions of permanganate gave the following absorbances (in a 1 cm cell): ABSORBANCE CONC. OF MnO4 (g/mL) 0.210 1.05 x 10-5 0.315 1.61 x 10-5 0.429 2.21 x 10-5 0.599 2.98 x 10-5 0.801 4.04 x 10-5 The following samples of steel were thoroughly reacted to convert the manganese ir permanganate and then diluted to 500.00 mL. WT. OF STEEL (g) ABSORBANCE 0.5886 0.611 0.3498 0.359 0.4555 0.482 Again using Excel, plot the calibration data and calculate the %Mn in the steel.
Chapter26: Molecular Absorption Spectrometry
Section: Chapter Questions
Problem 26.15QAP
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