A 0.5962 g sample of iron ore is dissolved in perchloric acid (HCIO4). All iron present is oxidized to Fe3*. The solution is filtered to remove solid matrix materials and made basic with addition of ammonium hydroxide. The iron precipitates as the Fe(OH)3.XH2O gel. The precipitate is collected in a cistern crucible and ignited to produce Fe203. What is the wt. % of iron in the sample if the analysis produced 0.3210 g Fe2O3? Fe3+ + 3 OH → Fe,O3 + → Fe203 H2 18.83% 9.415% 56.49% O 37.66%

Fundamentals Of Analytical Chemistry
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ISBN:9781285640686
Author:Skoog
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Chapter13: Titrations In Analytical Chemistry
Section: Chapter Questions
Problem 13.27QAP
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A 0.5962 g sample of iron ore is dissolved in perchloric acid (HCIO4). All iron present
is oxidized to Fe3*. The solution is filtered to remove solid matrix materials and made
basic with addition of ammonium hydroxide. The iron precipitates as the
Fe(OH)3.XH2O gel. The precipitate is collected in a cistern crucible and ignited to
produce Fe203. What is the wt. % of iron in the sample if the analysis produced
0.3210 g Fe2O3?
Fe3+ + 3 OH → Fe,O3 +
→ Fe203
H2
18.83%
9.415%
56.49%
O 37.66%
Transcribed Image Text:A 0.5962 g sample of iron ore is dissolved in perchloric acid (HCIO4). All iron present is oxidized to Fe3*. The solution is filtered to remove solid matrix materials and made basic with addition of ammonium hydroxide. The iron precipitates as the Fe(OH)3.XH2O gel. The precipitate is collected in a cistern crucible and ignited to produce Fe203. What is the wt. % of iron in the sample if the analysis produced 0.3210 g Fe2O3? Fe3+ + 3 OH → Fe,O3 + → Fe203 H2 18.83% 9.415% 56.49% O 37.66%
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