A 0.9092g sample of wheat flour was analyzed by Kjeldahl method. The ammonia formed was distilled into 50.00 mL of 0.05063 M HCl; a 7.46 mL back titration with 0.04917 M NaOH was required. Calculate the % protein in the flour. Input the value only. Express in 2 SF.
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- 2.) A 0.2185g sample of NaCl was assayed using Volhard Method with 50mL 0f 0.0998N AgNO3 and 11.9mL of 0.1350N NH4SCN. Calculate the % NaCl in the sample.A 1.5000-g sample of cereals was analyzed for nitrogen using the Kjeldahl procedure. The receiving flask contained 69 mL of 0.02 M HCl. After the ammonia was collected, the solution was titrated with 0 M NaOH, requiring 11.72 mL to reach the methyl red endpoint. Calculate and percent protein in the sample (f=5.70). Ans. in 3 SFs1. A 1.2-gram sample of lanolin was treated with Wij’s solution and excess potassium iodide solution. The liberated iodine reacted with 30 ml of 0.1 N sodium thiosulfate solution. If the iodine value was determined as 12.69, what is the volume used in blank titration? 2. A fat sample with combination of acids contain standard hydrochloric acid for blank and sample with 8mL and 5mL respectively. The normality of the standard hydrochloric acid is 0.93N and the weight of the sample is 3 grams. Calculate the saponification value. 3. A 3.50-gram sample of Streptomycin powder was tested for its water content. If the water equivalence factor of the KF reagent was 4.6, what is the percentage water content of the sample if 9.2 ml of the KF reagent was used? 4. A 500mg oil sample is taken from a conical flask and is dissolved in 50mL distilled alcohol. An indicator is added and is then titrated against 0.112N KOH until a slight pink color appears. It took 17.6mL of the titrant to reach the…
- An unknown sample of Cu2+gave an absorbance of 0.262. Then 1.00 mL of solution containing 100 ppm (ug/mL)Cu2+was mixed with 95.0 mL of the unknown and the mixture was diluted to 100 mL in a volumetric flask with deionized water. The absorbanceof the new solution was 0.500. a.Denoting the initial unknown concentrationas [Cu2+]i,write an expression for the final concentrationafter dilution [Cu2+] b.Find [Cu2+]in the unknown.A STOCK SOLUTION containing 0.1581 g/L K2CrO4 was prepared.In order to make the CALIBRATION STANDARD, 5 ml of the STOCK was transferredinto a 50ml volumetric flask and then diluted with an appropriate solvent.Calculate:(a) The ppm of K2CrO4 in the CALIBRATION STANDARD.(b) The molarity of K2CrO4 in the CALIBRATION STANDARD. (c) Calculate the molar absorptivity of K2CrO4 (at 371.0 nm). Assume that Beer's Law isobeyed over this concentration range.At 371.0 nm, this CALIBRATION STANDARD in a cell of path length 1.00 cm gave a %T of 59.752.Measure the mass of 0.400g of Co(NO3)2 + 6H2O and dissolve it in 15mL of distilled or deionized water using a clean beaker Then while using a graduated cylinder, measure out 10.0mL of a prepared 0.10-M Na3PO4 soultion. Determine which compound Na3PO4 or Co(NO3)2 *6H2O will be the limliting reagent. Then detrimine the theiretical yeild
- A mixture of pure BaCO3 and pure Na2CO3 weighs 1.000 g and has the total neutralizing power of 15.37 meq of CaCO3. Calculate the percentage of combined CO2 in the mixture and the weight of Li2CO3 that has the same neutralizing power as 1.000 g of the above mixture. Instructions: Include up to 4 decimal places See sample photo for the format of solutionZhongli is a speleologist tasked to analyze the CaCO₃ content of a limestone stalactite. A 5.0000-g sample was dissolved in 25.00 mL of 1.350 M HCl, it was then heated to expel any CO₂ formed. The excess HCl was titrated to a phenolphthalein end point, it used 37.50 mL of 0.1200 M NaOH. A. How many moles of HCl was added initially to digest the limestone sample? B. How many moles of CaCO₃ is present in the limestone sample? C. What is the purity of the limestone in terms of %w/w CaCO₃?The concentration of Cl– in a 300.0-mL sample of water drawn from a fresh water acquifer suffering from encroachment of sea water, was determined by titrating with 0.0516 M Hg(NO3)2. The sample was acidified and titrated to the diphenylcarbazone end point, requiring 6.18 mL of the titrant. Report the concentration of Cl–in parts per million
- The total cation content of natural water is often determined by exchanging the cations for hydrogen ions on a strong acid ion-exchange resin. A 25.00 mL sample of a natural water was diluted to 100.00 ML with distilled water, and 2.06 g of a cation - exchange resin was added. After stirring, the mixture was filtered and the solid remaining on the filter paper was washed with three 15.00 mL portions of water. The filtrate and washings required 16.30 mL of 0.0282 M NaOH to give a bromocresol green end point. a) Calculate the number of millimoles of cation present in exactly 1.00 L of sample. b ) Report the results in terms of milligrams of CaCO3 per liter. Only typed solution.You have to make 50 mL of 0.05M HCl from a 10M HCl stock solution, but the only measuring devices available are 100mL graduated cylinders and 10mL serological pipets. How could you accurately make the dilute HCl solution (clearly explain)?In one trial determination of the concentration of NaOCl in the diluted bleach sample, 10.00 mL of the diluted bleach solution required 23.32 mL of 0.0195 M Na2S2O3 titrant to reach the endpoint. What is the molar concentration of NaOCl in the diluted bleach solution?