A From the given spectral data, identiſy the compound and provide justífication for MS fragmentation, IR bands and identify the protons and provided NMR data : carbon from the Mol. formula :C5H100 Ms : m/z= 86 · 1, 71, 44 IR (liquid film) : 1728, 2822, 2960 (cm-1) 'H-NMR (8 : A =9.75, B =2:32, C=2.21, D=0.98 ppm

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter13: Mass Spectrometry
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A From the given spectral data, identiſy the
compound and provide justification for
MS fragmentation, IR bands and identify
the protons and carbon from the
provided NMR data :
Mol. formula : C5H100
Ms : m/z= 86· 1, 71, 44
IR (liquid film) : 1728, 2822,
2960 (cm-)
'H-NMR (8 : A =9.75, B = 2:32,
C=2.21, D =0-98 ppm
(suggest splitting pattern)
13 C-NMR (8 : (Proton decoupled)
1=202.71, 2 =52.66.
3 = 23-57, 4 =22-59
Transcribed Image Text:A From the given spectral data, identiſy the compound and provide justification for MS fragmentation, IR bands and identify the protons and carbon from the provided NMR data : Mol. formula : C5H100 Ms : m/z= 86· 1, 71, 44 IR (liquid film) : 1728, 2822, 2960 (cm-) 'H-NMR (8 : A =9.75, B = 2:32, C=2.21, D =0-98 ppm (suggest splitting pattern) 13 C-NMR (8 : (Proton decoupled) 1=202.71, 2 =52.66. 3 = 23-57, 4 =22-59
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