Acetylsalicylic acid commonly known as Aspirin is used to treat fever, inflammation, and acts as a blood thinning agent. A group of STEM students experimented on the synthesis of this compound using recrystallization technique. The following are the initial materials for the experiment: 5.00 g of pure salicylic acid, 7.14 g of acetic anhydride and 8 drops concentrated sulfuric acid as catalyst. After successful synthesis, the group was able to collect 5.25 grams of Aspirin. (Atomic weights: C= 12 amu; H = 1 amu; O= 16 amu; density acetic anhydride = 1.08 g/mL) Chemical reaction involved: OH -CH3 -CH3 с-он C-CH3 CH3-C-OH c-OH Acetic anhydride Salicylic acid (C7H603) Acetylsalicylic acid Acetic Acid (C 4H603) (C 9H804) (C 2 H402) low many molecules will be present in the Aspirin produced? 2.18 x1022 O 7.44 x1022 O 8.13 x1022 O 9.20 x1022

Acetylsalicylic acid commonly known as Aspirin is used to treat fever, inflammation, and acts as a blood thinning agent. A group of STEM students experimented on the synthesis of this compound using recrystallization technique. The following are the initial materials for the experiment: 5.00 g of pure salicylic acid, 7.14 g of acetic anhydride and 8 drops concentrated sulfuric acid as catalyst. After successful synthesis, the group was able to collect 5.25 grams of Aspirin. (Atomic weights: C= 12 amu; H = 1 amu; O= 16 amu; density acetic anhydride = 1.08 g/mL) Chemical reaction involved: OH -CH3 -CH3 с-он C-CH3 CH3-C-OH c-OH Acetic anhydride Salicylic acid (C7H603) Acetylsalicylic acid Acetic Acid (C 4H603) (C 9H804) (C 2 H402) low many molecules will be present in the Aspirin produced? 2.18 x1022 O 7.44 x1022 O 8.13 x1022 O 9.20 x1022

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter13: Isolation Of Eugenol From Clov

Section: Chapter Questions

Problem 9Q

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IDENTIFICATION: Acetylsalicylic acid commonly known as Aspirin (C9H8O4) is used to treat fever, inflammation, and acts as a blood-thinning agent. A group of STEM students experimented on the synthesis of this compound using recrystallization technique. The following are the initial materials for the experiment: 5.00 g of pure salicylic acid (C7H6O3), 7.14 g of acetic anhydride (C4H6O3) and 8 drops concentrated sulfuric acid as catalyst. After successful synthesis, the group was able to collect 5.25 grams of Aspirin (C9H8O4) and acetic acid (C2H4O2). Atomic weights: C= 12 amu; H = 1 amu; O= 16 amu; density acetic anhydride = 1.08 g/mL How much of the excess reactant (in grams) will be left unconsumed after the reaction?
A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted sample is transferred to the flask with a pipette, excess KI is added to it, and thus OCl- ion turns into Cl- ion and I2 is formed. The released iodine is titrated with 0.09892 Na2S2O3 using the starch reagent, and 8.96 mL is required for the endpoint. Find the % NaOCl (w/v; w/v) in the bleach sample. (Na=23 g/mol, O= 16 g/mol, Cl = 35.44 g/mol) (Warning: solving the necessary reaction equations by writing is necessary to see the stoichiometric relationship)
A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted sample is transferred to the flask with a pipette, excess KI is added to it, and thus OCl- ion turns into Cl- ion and I2 is formed. The released iodine is titrated with 0.09892 M Na2S2O3 using the starch reagent, and 8.96 mL is required for the endpoint. Find the % NaOCl (w/v; w/v) in the bleach sample. (Na=23 g/mol, O= 16 g/mol, Cl = 35.44 g/mol) (Warning: solving the necessary reaction equations by writing is necessary to see the stoichiometric relationship) A. 0.132% B. 0.264% C. 5.28% D. 10.56%
To synthesize methyl 3-nitrobenzoate, 20 ml of H2SO4 and 10 g of methyl benzoate were used. The nitrating mixture was prepared using 6 ml of H2SO4 and 6 ml of HNO3. Calculate the molar ratio of sulfuric acid to nitric acid
In the molecular weight determination by the Dumas method, several grams of an organic liquid was drawn into a bulb. The bulb was then immersed in a water bath at 87 degrees C and kept there until all the liquid was vaporized and the air in the bulb was replaced by the vapor. The tip was then sealed shut and the bulb removed from the vapor was 36.127g; the weight of the empty (evacuated) bulb was 35.427g; the bulb’s volume was 200.0mL; room temperature was 25 degrees C, and the barometric pressure was 720 mm Hg. Calculate the molecular weight of the organic liquid. Calculate the molecular weight of the organic liquid.
Cassava tuber has a composition of 5.76% moisture, 6% protein, 0.2% fat and 34.3 total carbohydrates, 1.6% fiber and 0.3% ash. Find the composition on dry basis.
2.1g of sample are dissolved in methylene chloride and the sample is extracted with aqueous solutions of acid and base. Three compounds are isolated - 0.8g of ethyl p-aminobenzoate, 0.6 g of acetanilide, and 0.5 g of benzoic acid. Calculate the % recovery for the procedure. (Round the answer to the nearest tens place.) Give just the number, not a % sign.)
A 0.9000-g of KIO3 is dissolved in 500-mL distilled water. A 50.0-mL aliquot portion was run down into an Erlenmeyer flask and 2-g of KI and 2-mL of 6M HCl were added to it. Directly after, the solution was titrated with a 24.80-mL Na2S2O3 solution to a faint yellow solution. Starch TS was added to the resulting solution and the titration with the Na2S2O3 solution continued wherein an additional 1.33-mL was required to bring the blue color of the solution to disappear completely. MW: KIO3 = 214.0 g/mol ; Na2S2O3 = 158.1 g/mol Compute the N of the Na2S2O3 solution. None of the choices 0.09657 N 0.1075 N 0.1017 N
ou separated acetanlide from sand and sodium chloride (NaCl) via recrystallization. You separated the recrystallized acetanilide from the dissolved NaCl using a seperatory funnel. You started the separation experiment with 4 g of an impure mixture of NaCl, sand, and acetanilide (MW= 135.17 g/mol) and you collected 3.2 g after the recrystallization experiment.Whats the percent yield?
In the industrial synthesis of aspirin, 200 kg of salicyclic acid, C7H6O3 and 150 kg of acetic anhydride (CH3CO)2O, form acetylsalicylic acid, C9H8O4, (aspirin) and acetic acid, C2H4O2. In a manufacturing process, 200 kg of aspirin are produced from 200 kg of impure salicyclic acid and 150 kg of acetic anhydride. The salicylic acid is the limiting reagent. Calculate the purity of the salicyclic acid. How many kg of excess reagent are left over, assuming there are no side reactions between the impurities in the limiting reagent and the excess reagent?
A 0.9134-g of KIO3 is dissolved in 500-mL distilled water. A 50.0-mL aliquot portion was run down into an Erlenmeyer flask and 2-g of KI and 2-mL of 6M HCl were added to it. Directly after, the solution was titrated with a 24.47-mL Na2S2O3 solution to a faint yellow solution. Starch TS was added to the resulting solution and the titration with the Na2S2O3 solution continued wherein an additional 1.33-mL was required to bring the blue color of the solution to disappear completely. MW: KIO3 = 214.0 g/mol ; Na2S2O3 = 158.1 g/mol Compute the M of the Na2S2O3 solution. 0.1047 M None of the choices 0.1107 M 0.09926 M
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