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- When warmed in dilute sulfuric acid, 1-phenyl-1,2-propanediol undergoes dehydration and rearrangement to give 2-phenylpropanal. (a) Propose a mechanism for this example of a pinacol rearrangement (Section 10.7). (b) Account for the fact that 2-phenylpropanal is formed rather than its constitutional isomer, 1-phenyl-1-propanone.Match the drugs with the corresponding Phase 1 reaction that will happen appropriately with the highligthed portion of the drug. A: C4 of Benzene ring B: Methyl group of Nitrogen C: -NH-NH2 moiety D: N,N-dimethyl moiety E: Ring S CHOICES: A. Desulfuration B. Aromatic hydroxylation C. Hydrazo reduction D. Nitro reduction E. Sulfur oxidation F. Deamination G. N-demethylation1. Show examples and structures the order of reactivity in SN2? 2. Show some SN2 reactions with Bromo-Ethene. Give 9 examples of Nucleophiles Nu- 3. Rank the following compounds in order of their expected reactivity toward SN2 reaction CH3Br, CH3OTos, (CH3)2CHCI 4. Show with examples for the influence of solvents in the SN2 reaction. 5. Show the Mechanism of the SN1 Reaction with the proper Directions of the arrows?
- 9. Product of the reaction of nitrobenzene with sulfuric acid in the presence of oleum at 60 °C:a) o-nitro benzenesulfonic acidb) m-nitro benzenesulfonic acidc) p-nitro benzenesulfonic acidd) None of the above 10. Due to their ability to move through ducts or pipes, they are generally called fluids:a) Solidsb) Solid mixturesc) Gasesd) Liquids and gasesA key step in the synthesis of naproxen, an NSAID more commonly known by its brand name, Aleve (Section 3.9), is a coupling reaction of 2-bromo-6-methoxynaphthalene to form 2-methoxy-6-vinylnaphthalene. Show three different coupling reactions, and the required reagents, that could be used tocarry out this step.Choose the best reagents from the list provided below for carrying out the following conversion. Match the reagent with the step number. HCl (aq), Zn(Hg) Br2, FeBr3 Na/NH3, -33 degrees C NBS, light KMnO4, H3O+ Mg metal, ether KOH, EtOH, heat
- ) Draw all the Kekulé structures of anthracene and phenanthrene.(b) Propose mechanisms for the two additions shown.(c) In Chapter 8, most of the additions of bromine to double bonds gave entirely antistereochemistry. Explain why the addition to phenanthrene gives a mixture of synand anti stereochemistry.(d) When the product from (c) is heated, HBr is evolved and 9-bromophenanthrene results.Propose a mechanism for this dehydrohalogenationWhat is reaction 1 and 2 called? Choices: A. Williamson ether synthesis, B. Reduction with Grignard reagent, C. Acidic ether cleavage, D. FC Alkylation What are the reagents for reaction 1 and 2? Choices: A. methanol in acidic medium, B. sodium hydride and bromomethane, C. methyl bromide and aluminum bromide, D. methanoyl bromidet-butyl bromide (2-bromo-2-methylpropane) undergoes an SN1 reaction (with solvent as nucleophile) in isopropyl alcohol/water mixtures. Isopropyl alcohol = CH3-CH(OH)-CH3; water = H2O; Given: water is more polar solvent than isopropyl alcohol. In which of the following solvent mixtures will t-butyl bromide react the fastest? Select one: A.50% isopropyl alcohol / 50% water B.40% isopropyl alcohol / 60% water C.70% isopropyl alcohol / 30% water D.30% isopropyl alcohol / 70% water
- draw 2 potential mechanisms for the etherification of ethyl vanillyl alcohol (3-ethoxy-4-hydroxybenzyl alcohol) with methanol and acid (Amberlyst® 15 resin): Sn1 and Sn2, complete with structures and arrows.one of the reaction mechanisms above involves a resonance stabilized carbocation. Draw all resonance structures for this carbocation.Provide a detailed, stepwise mechanism for the acid-catalyzed reaction of 2-butanone with ethylene glycol to produce an acetal. Problem 4. Show how 2-butanone could be prepared by a procedure in which all of the carbons originated in acetic acid, CH3 Problem 5. A compound has a molecular formula of C8H8O The following spectra (1H NMR, Carbon 13 NMR, IR was collected. Give a possible structure. 13C NMR – 8 peaksCombinatorial synthesis. comment on the below compounds features in relation to the structure-activity relationship (SAR). A5-B1 = 2-hydroxybenzaldehyde - 4-bromophenylhydrazine hydrochloride. A8-B1 = benzaldehyde - 4-bromophenylhydrazine hydrochloride.