Attached 1st Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found?  Peak Position cm-1 Bond Type Functional Group

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
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Chapter29: Mass Spectrometry
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Problem 29.4QAP
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Attached 1st Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found? 

Peak Position cm-1

Bond Type

Functional Group

     
     
     
     
     
     
     
     
     
     
Wavenumbers (cm-1)
4000
3500
3000
2500
2000
1500
1000
500
-2
0
$34.97
N
4
6
1248.08
8
10
12-
14-
16
18
20
22-
24
26
1678.11
1503.63
1487.15
1440.18
%Transmittance
1038.47
2977.99
2905.83
1604.99
1359.44
1140.00
1112.25
933.58
877.83
794.48
1460.69
1765.04
3077.21
3344.59
966.30
3224.27
2784.35
2717.68
2673.35
2616.36
2480.21
1859.63
1818.47
1308.71
1071.24
744.04 718.36
Transcribed Image Text:Wavenumbers (cm-1) 4000 3500 3000 2500 2000 1500 1000 500 -2 0 $34.97 N 4 6 1248.08 8 10 12- 14- 16 18 20 22- 24 26 1678.11 1503.63 1487.15 1440.18 %Transmittance 1038.47 2977.99 2905.83 1604.99 1359.44 1140.00 1112.25 933.58 877.83 794.48 1460.69 1765.04 3077.21 3344.59 966.30 3224.27 2784.35 2717.68 2673.35 2616.36 2480.21 1859.63 1818.47 1308.71 1071.24 744.04 718.36
Reaction 1
da
CH₁
ZnO (nanoparticles)
Heat
ol
CH₂
Transcribed Image Text:Reaction 1 da CH₁ ZnO (nanoparticles) Heat ol CH₂
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