13CNMR for unknown Z 120 110 100 90 80 70 60 50 40 30 20 10 0 199.00 210 ANKARA 200 190 180 170 160 150 127.45 127.97 131.80 136.90 140 FITTE 130 120 110 100 90 80 70 60 50 31.00 7.50 11 Page 9 of 9 40 30 20 10 0 11.5 11.0 10.55 10.0 95 9.0 85 8.0 7.5 70 6.53 6.0 5.55 5.0 4.5 403 3.5 3.0 25 20 153 1.0 0.5 0.0 8.0 TTT 7.5 7.0 6.5 6.0 HNMR for unknown Z, T 5.5 5.0 4.5 3.5 3.0 2.5 Page 8 of 9 2.0 1.5 10

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter32: Radiochemical Methods
Section: Chapter Questions
Problem 32.13QAP
icon
Related questions
Question

Spectra data for Unknown Z are listed below. Deduce it's structure. 
MS: m/z 134 (Molecular Ion) IR: 1720 (strong); 3062 (weak); 2981 (medium); 1605 (medium) 

13C NMR and 1H NMR shown on a separate page. 

13CNMR for unknown Z
120
110
100
90
80
70
60
50
40
30
20
10
0
199.00
210
ANKARA
200
190
180
170
160
150
127.45
127.97
131.80
136.90
140
FITTE
130
120
110
100
90
80
70
60
50
31.00
7.50
11
Page 9 of 9
40
30
20
10
0
Transcribed Image Text:13CNMR for unknown Z 120 110 100 90 80 70 60 50 40 30 20 10 0 199.00 210 ANKARA 200 190 180 170 160 150 127.45 127.97 131.80 136.90 140 FITTE 130 120 110 100 90 80 70 60 50 31.00 7.50 11 Page 9 of 9 40 30 20 10 0
11.5
11.0
10.55
10.0
95
9.0
85
8.0
7.5
70
6.53
6.0
5.55
5.0
4.5
403
3.5
3.0
25
20
153
1.0
0.5
0.0
8.0
TTT
7.5
7.0
6.5
6.0
HNMR for unknown Z,
T
5.5
5.0
4.5
3.5
3.0
2.5
Page 8 of 9
2.0
1.5
10
Transcribed Image Text:11.5 11.0 10.55 10.0 95 9.0 85 8.0 7.5 70 6.53 6.0 5.55 5.0 4.5 403 3.5 3.0 25 20 153 1.0 0.5 0.0 8.0 TTT 7.5 7.0 6.5 6.0 HNMR for unknown Z, T 5.5 5.0 4.5 3.5 3.0 2.5 Page 8 of 9 2.0 1.5 10
Expert Solution
steps

Step by step

Solved in 5 steps with 2 images

Blurred answer
Knowledge Booster
Quality Assurance and Calibration Methods
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning