Complete the following NMR peak assignment tables. Predict the chemical shifts, the splitting (multiplicity) pattern, and integration for compound A - D. The chemical environments of different Hs in each molecule are labeled and assigned. Use the H-NMR peak reference chart to predict the correct chemical shift values. First two rows in table 01 is done for you as an example. Ho He Hc Ho Ho Ha Ha He Ha Ha Compund A Table 01: Predicted NMR peak assignments data for compound A Predicted Predicted Type of chemical Chemical shift multiplication/splitting value (ppm) Predicted Peak integration Assignment environment pattern 3H 0.5 – 1.5 Triplet (t) H, C-CH3 2H 3.5 – 4.5 Quartet (q) H, H-C-O H. H. H,

Organic Chemistry: A Guided Inquiry
2nd Edition
ISBN:9780618974122
Author:Andrei Straumanis
Publisher:Andrei Straumanis
ChapterL3: Carbon (13c) Nmr Spectroscopy
Section: Chapter Questions
Problem 11E
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Ha Ha
Hayla
Ho
Ho.
Ha
Ho
Ha
На На
Compund B
Table 02: Predicted NMR peak assignments data for compound
В
Predicted
Predicted
Predicted
Type of chemical Chemical shift multiplication/splitting
value (ppm)
integration
Peak
environment
pattern
Assignment
H,
H,
H.
Transcribed Image Text:Ha Ha Hayla Ho Ho. Ha Ho Ha На На Compund B Table 02: Predicted NMR peak assignments data for compound В Predicted Predicted Predicted Type of chemical Chemical shift multiplication/splitting value (ppm) integration Peak environment pattern Assignment H, H, H.
Complete the following NMR peak assignment tables. Predict
the chemical shifts, the splitting (multiplicity) pattern, and
integration for compound A - D. The chemical environments of
different Hs in each molecule are labeled and assigned.
Use the H-NMR peak reference chart to predict the correct
chemical shift values.
First two rows in table 01 is done for you as an example.
Ho
He
Hc
Ho
Ho
Ha
На
He
Ha
Ha
Compund A
Table 01: Predicted NMR peak assignments data for compound
A
Predicted
Predicted
Type of chemical Chemical shift multiplication/splitting
value (ppm)
Predicted
Peak
integration
Assignment
environment
pattern
3H
0.5 – 1.5
Triplet (t)
H,
C-CH3
2H
3.5 – 4.5
Quartet (q)
H,
H-C-O
H.
H.
H,
Transcribed Image Text:Complete the following NMR peak assignment tables. Predict the chemical shifts, the splitting (multiplicity) pattern, and integration for compound A - D. The chemical environments of different Hs in each molecule are labeled and assigned. Use the H-NMR peak reference chart to predict the correct chemical shift values. First two rows in table 01 is done for you as an example. Ho He Hc Ho Ho Ha На He Ha Ha Compund A Table 01: Predicted NMR peak assignments data for compound A Predicted Predicted Type of chemical Chemical shift multiplication/splitting value (ppm) Predicted Peak integration Assignment environment pattern 3H 0.5 – 1.5 Triplet (t) H, C-CH3 2H 3.5 – 4.5 Quartet (q) H, H-C-O H. H. H,
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