Determination of melting point can also be done by heating melting point capillary to the thermometer using “Thiele tube”. Draw a complete Thiele tube melting point apparatus. What effect would poor circulation of the melting point bath liquid have on the observed melting point?

Determination of melting point can also be done by heating melting point capillary to the thermometer using “Thiele tube”. Draw a complete Thiele tube melting point apparatus. What effect would poor circulation of the melting point bath liquid have on the observed melting point?

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter33: Automated Methods Of Analysis

Section: Chapter Questions

Problem 33.8QAP

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Question

Determination of melting point can also be done by heating melting point capillary to the thermometer using “Thiele tube”. Draw a complete Thiele tube melting point apparatus. What effect would poor circulation of the melting point bath liquid have on the observed melting point?

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