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- Pyrolusite (MnO2) is dissolved in hydrochloric acid:MnO2 + HCl → MnCl2 + H2O + Cl2The chloride was passed into potassium iodide solution where it liberated iodine:Cl2 + KI → KCl + I2The iodine liberated was estimated by adding sodium thiosulfate, the reaction beingI2 + Na2S2O3 → NaI + Na2S4O6If 5.6 g of crystallized sodium thiosulfate, Na2S2O3 5H2O ,were used up, how many grams of manganese were present?MW (g/mole): I =126.9; Mn =54.94; Cl = 35.45; K = 39.09; Na = 23; S = 32Given A, B, and C… [A] U(VI) as uraninite; UO2 (where Fe2+= reductant; Fe(OH)3 ferrihydrite= product): 2Fe2+ + UO22+ +3H2O + H+ ---- > 2Fe(OH)3 + U4+ +2H2O [B] U(VI) as uraninite; UO2 (where Mn2+= reductant; MnO2 pyrolusite= product): 2H2O + UO22+ + Mn2+ ---- > UO2 + B - MnO2 + 4H+ [C] U(VI) as as uraninite; UO2 (where HS-= reductant; S0= product): UO22+ + Hs- ---- > UO2 + S + H+ QUESTION: Use thermodynamic calculations [use redox potential (Eh)] to predict which of the three reductants below is most favorable at pH 3 ? (1) Fe2+ (2) Mn2+ (3) HS-What is the percentage of Nickel in an ore if, when analyzed by the cyanide method, 20.00mL of KCN solution (containing 1.00mmol of AgNO3 per milliliter) are used? Wt of sample used = 0.2500g
- How many milliliters of 1.5% alcoholic dimethylglyoxime should be used to provide a36.0% excess with 0.6984 q of steel containing 2.95 wt% Ni? Assume that the densityof the dimethylglyoxime solution is 0.790 g/mL. a. How much Ni sample is present? b. How many moles Ni is present in the sample? c. How much DMG is present?1. A Cr3+ solution is electrolyzed using a current of0.365 A. What mass of Cr(s) (51.9661) is plated outafter 10 hours?2. When an aqueous solution of CuSO4 is electrolyzedcopper metal is deposited. If a constant current waspassed for 5.00 h and 404 mg of Cu (63.546) metal wasdeposited, what was the current?what wt. of limestone containing 9.57% Mg must be taken for analysis in order to precipitate of 0.551g Mg2P2O7? how many grams of Na2SO4 are required to ppte Ag2SO4 from 2.000t of AgNO3? a sample of magnetite (impure Fe3O4) weighing 0.5000g is fused with oxidizing flux and the ferric compound formed is eventually precipitated as ferric hydroxide and ignited to ferric oxide which weighs 0.4980calculate %Fe & %Fe2O3
- The thickness of the chromium plate on an auto fender is determined by dissolving a 30.0-cm2section in acid and oxidizing Cr3+ to Cr2O72-with peroxydisulfate. After removing excess peroxydisulfate by boiling, 500.0 mg of Fe(NH4)2(SO4)2•6H2O is added, reducing the Cr2O72-to Cr3+. The excess Fe2+ is back titrated, requiring 18.29 mL of 0.00389 M K2Cr2O7 to reach the end point. Determine the average thickness of the chromium plate given that the density of Cr is 7.20 g/cm3. Note: thickness = volume /areaLike heavy water (D₂O), so-called “semi-heavy water”(HDO) undergoes H/D exchange. The scenes below depict aninitial mixture of HDO and H₂ reaching equlibrium.(a) Write the balanced equation for the reaction. (b) Is the valueof Kgreater or less than 1? (c) If each molecule depicted repre-sents 0.10 M, calculate K.(a) What is the percentage of MnO2 in a pyrolusite ore if a sample weighing 0.4000g is treated with 0.6000g of pure H2C2O4•2H2O and dilute H2SO4 and after reduction has taken place (MnO2 + H2C2O4 + 2H+→ Mn2++ 2CO2 + 2H2O), the excess oxalic acid requires 26.26ml of 0.1000N KMnO4 for titration? (b) If pure As2O3 were used instead of oxalic acid, how many grams would be required in order for the other numerical data to remain the same?
- A sample of iron ore weighing 800 mg was treated with HNO3 , boiled to dryness and redissolved in dilute HCl. After filtration and removal of undissolved silica, the liquid was passed through a Walden reductor. The collected sample was titrated with 0.0210 M KMnO4 , requiring 12.0 mL to reach the end point. Calc %Fe (55.845) in the ore.Pyrite (FeS2) is often roasted to obtain sulfur dioxide for making sulfuric acid. Consider the roasting reactionFeS2 + O2 = Fe2O3 + SO2Stoichiometric exercises:a) Formulate the correct stoichiometric roasting reaction Calculate, in respect to 1 t of pyrite, the stoichiometric amounts ofb) Oxygen required for roasting (in m3) c) Obtained hematite by-product (in t) d) Sulfur dioxide produced (in m3) Thermodynamic considerations:e) Calculate the reaction enthalpy ∆Ho298 for the above roasting reaction (in MJ/t of pyrite) Mind you: Requested is the reaction enthalpy per 1 t of pyrite! f) State whether the reaction is exo- or endothermic and say why. g) Calculate the actual change of entropy ∆So298 in J/(mol K) and explain why it is positive or negativePercentage purity of a sample of 0.1350 g of As2O3 assayed iodometrically using 23.5 mL of 0.1055N iodine solution