Elucidate the structure for compound Busing spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D2O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (iii) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%) ; 87 (0.5); 68.07 (100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J = 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet), 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) LOD 4000 3000 2000 HAVENUMBERI-1 1500 1000 500
Elucidate the structure for compound Busing spectroscopic data provided. B. Spectral analysis of a pure compound gave the following MS, IR data and H-NMR data (after D2O shake). i) Provide the Molecular formula, (ii) Identify the correct structure (iii) Identify the most important (diagnostic) IR signal(s) and match each proton NMR absorption with the proton that is causing that absorbance? MS: m/z: 86 (10%) ; 87 (0.5); 68.07 (100.0%), 69.08 (5.4%) 1H NMR (d): 5.67 (1H, doublet, J = 18), 5.63 (1H, quartet, J= 17), 4.38 (1H, quartet), 1.63 (3H, doublet), 1.07 (3H, doublet). IR (see below) LOD 4000 3000 2000 HAVENUMBERI-1 1500 1000 500
Chapter12: Structure Determination: Mass Spectrometry And Infrared Spectroscopy
Section12.SE: Something Extra
Problem 48AP: The infrared spectrum of the compound with the mass spectrum shown below lacks any significant...
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