Following a reaction period of 150-minutes, you decide to perform an extraction to eliminate any triethylammonium chloride salts that formed as well as any potential remaining starting materials. You transfer the reaction mixture to a separatory funnel and add distilled water. Identify the layers in the separatory funnel. O The top layer is the aqueous layer, and the bottom layer is the organic layer. O The top layer is the organic layer, and the bottom layer is the aqueous layer. O DCM and water are miscible solvents, and no layers form. Performing an extraction was a mistake. A distillation should have been used to purify the desired material.

Organic Chemistry: A Guided Inquiry
2nd Edition
ISBN:9780618974122
Author:Andrei Straumanis
Publisher:Andrei Straumanis
Chapter20: Acidity And Pka Of Phenols
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QUESTION 5
Following a reaction period of 150-minutes, you decide to perform an extraction to eliminate any triethylammonium
chloride salts that formed as well as any potential remaining starting materials. You transfer the reaction mixture to a
separatory funnel and add distilled water. Identify the layers in the separatory funnel.
The top layer is the aqueous layer, and the bottom layer is the organic layer.
The top layer is the organic layer, and the bottom layer is the aqueous layer.
DCM and water are miscible solvents, and no layers form.
Performing an extraction was a mistake. A distillation should have been used to purify the desired material.
O O
Transcribed Image Text:QUESTION 5 Following a reaction period of 150-minutes, you decide to perform an extraction to eliminate any triethylammonium chloride salts that formed as well as any potential remaining starting materials. You transfer the reaction mixture to a separatory funnel and add distilled water. Identify the layers in the separatory funnel. The top layer is the aqueous layer, and the bottom layer is the organic layer. The top layer is the organic layer, and the bottom layer is the aqueous layer. DCM and water are miscible solvents, and no layers form. Performing an extraction was a mistake. A distillation should have been used to purify the desired material. O O
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