How many 1H-NMR and 13C-NMR resonance signals would you expect in each spectrum for 2-aminophenyl phenyl sulfide?

Organic Chemistry
8th Edition
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Chapter13: Nuclear Magnetic Resonance Spectroscopy
Section: Chapter Questions
Problem 13.28P
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How many 1H-NMR and 13C-NMR resonance signals would you expect in each spectrum for 2-aminophenyl phenyl sulfide?

180
160
140
120
100
80
60
40
20
ppm
Ppm
Int. Assign.
148.82
137
1
NH,
137.44
529
167
2
3
136.83
$19
128.98 1000
131.10
126.5e
956
125.40
118.72
553
7
550
115.34
482
9
114.41
105
10
Transcribed Image Text:180 160 140 120 100 80 60 40 20 ppm Ppm Int. Assign. 148.82 137 1 NH, 137.44 529 167 2 3 136.83 $19 128.98 1000 131.10 126.5e 956 125.40 118.72 553 7 550 115.34 482 9 114.41 105 10
NH2
7
5.
4.
2
1.
Assign.
Shift(ppm)
H
H
H
7.447
7.22
7.21
7.10
H
7.09
6.77
6.75
4.27
H
Ha HE
Peaks B and C overlapped to the solvent peak. The
solvent peak was not deleted fron this spectrum.
Transcribed Image Text:NH2 7 5. 4. 2 1. Assign. Shift(ppm) H H H 7.447 7.22 7.21 7.10 H 7.09 6.77 6.75 4.27 H Ha HE Peaks B and C overlapped to the solvent peak. The solvent peak was not deleted fron this spectrum.
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