H NMR ppm C NMR DEPT - 135 DEPT - 90 Solvent 180 160 140 120 100 80 60 40 20 ppm

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter34: Particle Size Determination
Section: Chapter Questions
Problem 34.9QAP
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Question

Predict the structure of the compound using the information below. Kindly show what information are obtained for each spectra which may help in predicting the structure.

  • From IR Spectra: See the attached picture
  • From Mass Spectra:
    • M+ = 216
    • peaks at 29 (base peak) and 188
  • From Proton and Carbon NMR Spectra: See attached picture.
IR Spectra
LOD
50
4000
3000
2000
1500
1000
NAVENUMBERI
TPANSMITTANCEIXI
Transcribed Image Text:IR Spectra LOD 50 4000 3000 2000 1500 1000 NAVENUMBERI TPANSMITTANCEIXI
H NMR
2
ppm
C NMR
DEPT - 135
DEPT - 90
Solvent
180
160
140
120
100
80
60
40
20
ppm
Transcribed Image Text:H NMR 2 ppm C NMR DEPT - 135 DEPT - 90 Solvent 180 160 140 120 100 80 60 40 20 ppm
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