In Aspirin lab preparation a student used 69.0 g of salicylic acid and 30.0 g of acetic anhydride. Write the general balanced equation and calculate the reaction efficiency, if the pure aspirin was 0.25 mole. Why did you use phosphoric acid in the reaction?

In Aspirin lab preparation a student used 69.0 g of salicylic acid and 30.0 g of acetic anhydride. Write the general balanced equation and calculate the reaction efficiency, if the pure aspirin was 0.25 mole. Why did you use phosphoric acid in the reaction?

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter39: Preparation Of An Α, Β-unsaturated Ketone Via Michael And Aldol Condensation Reactions

Section: Chapter Questions

Problem 2Q

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In Aspirin lab preparation a student used 69.0 g of salicylic acid and 30.0 g of
acetic anhydride. Write the general balanced equation and calculate the reaction
efficiency, if the pure aspirin was 0.25 mole. Why did you use phosphoric acid in
the reaction?

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Aspirin can be made in the laboratory by reacting acetic anhydride (C4H6O3C4H6O3) with salicylic acid (C7H6O3C7H6O3) to form aspirin (C9H8O4C9H8O4) and acetic acid (C2H4O2C2H4O2). The balanced equation isC4H6O3+C7H6O3→C9H8O4+C2H4O2C4H6O3+C7H6O3→C9H8O4+C2H4O2In a laboratory synthesis, a student begins with 3.10 mLmL of acetic anhydride (density=1.08gml−1density=1.08gml−1) and 1.23 gg of salicylic acid. Once the reaction is complete, the student collects 1.22 gg of aspirin. Determine the percent yield of aspirin for the reaction. Express your answer using three significant figures.
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