Match Column A with Column B. uses a graphite-coated furnace to vaporize the sample A. GFAAS samples are deposited in a pyrolytic coated graphite tube B. Cold vapor technique used in direct analysis of solid samples and slurry materials C. Hydride generation technique
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- Calculate the time, in minutes, needed to plate 17.697 g of metal M at 43 Amps. The molar mass of metal M is 57.915 g/mol. M6+ + 6 e– → M Recall that, C = A*s, and Faraday’s constant, F, is 96,485 C/mole of electrons.What is the Electrolysis industrial chemical process, (and write a half-page summary of it in 12pt font, single-spaced). Explain what is produced, the chemical reaction(s) involved, why this process/product is important, and how an understanding of limiting reagents is important in optimizing this process. Use at least two sources of information. Provide URLs for all sources you use in your research. Chemical reactions discussed must be complete and balanced, including states.A 100 ml sample of pond water was analyzed using Winkler method to determine its oxygen demand. It took 32.4 ml of 0.0100 M Na2S2O3 to react with Iodine. Calculate the oxygen for this pond water.
- Explain passivation by drawing hypothetical polarization curve and which parameters have effects on the passivity of a metal and the corrosivity of an electrolyte. Show reaction steps for a nickel oxide passive filmFor Redox Analysis of Iron... ~0.02 M of potassium dichromate is prepared as titrant for dried unknown. ~.3 g of sample, 50ml of 6M HCl, 20mL SnCl2, 10 mL of saturated HgCl2 solution, 60 mL of 3M H2SO4, 15mL of concentrated H3PO4, 100mL DI water. HCl (+ heat in fumehood until samples dissolves), SnCl2 (added with pipet until solution changes from yellow to colorless/light green with 3 drops in excess), HgCl2 (after cooling), H2SO4, H3PO4, DI Water, is added to the sample solution with 8 drops of diphenylamine sulfonate indicator then titrated with the potassium dichromate to a violet blue endpoint. 4. Why is it necessary to carry out the reduction of iron and then the titration, before going on to the next sample 5. If you look carefully, there are pieces of tin metal on the bottom of the SnCl2 reagent solution. Why is it there?For Redox Analysis of Iron... ~0.02 M of potassium dichromate is prepared as titrant for dried unknown. ~.3 g of sample, 50ml of 6M HCl, 20mL SnCl2, 10 mL of saturated HgCl2 solution, 60 mL of 3M H2SO4, 15mL of concentrated H3PO4, 100mL DI water. HCl (+ heat in fumehood until samples dissolves), SnCl2 (added with pipet until solution changes from yellow to colorless/light green with 3 drops in excess), HgCl2 (after cooling), H2SO4, H3PO4, DI Water, is added to the sample solution with 8 drops of diphenylamine sulfonate indicator then titrated with the potassium dichromate to a violet blue endpoint. 1. What is the purpose of the phosphoric acid in this experiment? Please be specific. 2. How does the Diphenylamine sulfonate indicator work? What chemical reaction causes the color change? How is an indicator chosen in a redox reaction?
- For Redox Analysis of Iron... ~0.02 M of potassium dichromate is prepared as titrant for dried unknown. ~.3 g of sample, 50ml of 6M HCl, 20mL SnCl2, 10 mL of saturated HgCl2 solution, 60 mL of 3M H2SO4, 15mL of concentrated H3PO4, 100mL DI water. HCl (+ heat in fumehood until samples dissolves), SnCl2 (added with pipet until solution changes from yellow to colorless/light green with 3 drops in excess), HgCl2 (after cooling), H2SO4, H3PO4, DI Water, is added to the sample solution with 8 drops of diphenylamine sulfonate indicator then titrated with the potassium dichromate to a violet blue endpoint. 3. How would you prepare a complete anlaysis procedure using KMnO4 as the oxidant instead of K2CrO7? Include sample and solution preparation, approximate weights of samples and reagents, procedure and chemical reactions. In particular what is the purpose of the Zimmerman Reinhardt Reagent?Pyrolusite (MnO2) is dissolved in hydrochloric acid:MnO2 + HCl → MnCl2 + H2O + Cl2The chloride was passed into potassium iodide solution where it liberated iodine:Cl2 + KI → KCl + I2The iodine liberated was estimated by adding sodium thiosulfate, the reaction beingI2 + Na2S2O3 → NaI + Na2S4O6If 5.6 g of crystallized sodium thiosulfate, Na2S2O3 5H2O ,were used up, how many grams of manganese were present?MW (g/mole): I =126.9; Mn =54.94; Cl = 35.45; K = 39.09; Na = 23; S = 32Iron corrodes to produce rust, Fe2O3, but other corrosionproducts that can form are Fe(O)(OH), iron oxyhydroxide,and magnetite, Fe3O4. (a) What is the oxidation numberof Fe in iron oxyhydroxide, assuming oxygen’s oxidationnumber is -2? (b) The oxidation number for Fe in magnetitewas controversial for a long time. If we assume thatoxygen’s oxidation number is - 2, and Fe has a uniqueoxidation number, what is the oxidation number for Fein magnetite? (c) It turns out that there are two differentkinds of Fe in magnetite that have different oxidationnumbers. Suggest what these oxidation numbers are andwhat their relative stoichiometry must be, assuming oxygen’soxidation number is -2.
- Knowing that an electroplating industry wants to recover a steel sheet with a layer of metallic Ni through an electrodeposition process, answer the items below:a) What is the cathode material and what materials could be used as anode (cite at least 2). justify yourchoice.b) what are the constituents of an electroplating bath (solution)?c) what are the main stages for the production of a part for an electroplating coating?d) what is the time in hours to deposit a 65 µm layer on a 1 m2 plate (both sides) applying a current density of 35 mA/cm2 if the process efficiency is 75%.Data MM Ni= 58.69 g/mol and d= 8.92 g/cm3Impure nickel, refined by smelting sulfide ores in a blast furnace, can be convertedinto metal from 99.90% to 99.99% purity by the Mond process. The primaryreaction involved in the Mond process is:Ni(s) + 4CO(g) ⇌ Ni(CO)4(g)In the second step of the Mond process, the gaseous Ni(CO)4 is isolated andheated to 227°C. The purpose of this step is to deposit as much nickel as possibleas pure solid (the reverse of the preceding reaction). Calculate the equilibriumconstant for the preceding reaction at 227°C.A steel sheet will have a thin layer of zinc put on one side to protect it from corrosion. Determination of the zinc film thickness per one centimeter square of steel sheet when a 2 A current is employed and the electrolytic deposition process is completed in exactly 30 minutes at 25 degrees Celsius. With a 1 M zinc solution, it's safe to presume that its concentration will remain stable throughout the process.