Na₂SO4 xH₂O Which best fits in blank 7? 4-methylacetophenone methylene chloride trace toluene 4-methylacetophenone boil off solvent cool in ice bath anhydrous sodium sulfate reflux for 30 minutes 7) g 8) trace toluene

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter7: Extraction
Section: Chapter Questions
Problem 1Q
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S
Na₂SO4-xH₂O
Which best fits in blank 7?
organic
4-methylacetophenone
methylene chloride
trace toluene
trace water
reflux for 30 minutes
trace 3)
boil off solvent
cool in ice bath
anhydrous sodium sulfate
4-methylacetophenone
extract with aqueous
4).
4-methylacetophenone
methylene chloride
trace toluene
7)
aq
5)_
sodium chloride
water
CO₂(g)
8
8)
trace toluene
Transcribed Image Text:S Na₂SO4-xH₂O Which best fits in blank 7? organic 4-methylacetophenone methylene chloride trace toluene trace water reflux for 30 minutes trace 3) boil off solvent cool in ice bath anhydrous sodium sulfate 4-methylacetophenone extract with aqueous 4). 4-methylacetophenone methylene chloride trace toluene 7) aq 5)_ sodium chloride water CO₂(g) 8 8) trace toluene
For question below the separation scheme, please indicate the compound that best
fits in the blank of the separation scheme . Hint: s = solid, I = liquid, g = gas and aq
aqueous.
4-methylacetophenone
soluble aluminum salt (A1C13 destroyed by aqueous HC1)
acetic acid (from any unreacted acetyl chloride)
trace toluene
hydrochloric acid
water
methylene chloride
aq
soluble aluminum salt
acetic acid
hydrocholic acid
water
multiple Extractions with water and methylene chloride
organic
4-methylacetophenone
methylene chloride
trace toluene
trace acetic acid, and H₂O
trace 3)
organic
4-methylacetophenone
methylene chloride
trace toluene
trace water
extract with aqueous
aq
5)
sodium chloride
water
CO₂(8)
Transcribed Image Text:For question below the separation scheme, please indicate the compound that best fits in the blank of the separation scheme . Hint: s = solid, I = liquid, g = gas and aq aqueous. 4-methylacetophenone soluble aluminum salt (A1C13 destroyed by aqueous HC1) acetic acid (from any unreacted acetyl chloride) trace toluene hydrochloric acid water methylene chloride aq soluble aluminum salt acetic acid hydrocholic acid water multiple Extractions with water and methylene chloride organic 4-methylacetophenone methylene chloride trace toluene trace acetic acid, and H₂O trace 3) organic 4-methylacetophenone methylene chloride trace toluene trace water extract with aqueous aq 5) sodium chloride water CO₂(8)
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