The workup of preparation of 1-bromobutane involves pouring the distillate into a separatory funnel and shaking with about 10 mL of water. Jesse observes the lower 1-bromobutane layer has a pink coloration. This is due to presence o Brg. Suggest how Jesse can rectify this. O Add a pinch of sodium bisulfite, NAHSO3. O Rinse the 1-bromobutane layer with another portion of water. Add a scoop of anhydrous CaCl2. Add 10 ml. of cold concentrated H2S04-

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter4: Recrystallization
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The workup of preparation of 1-bromobutane involves pouring the distillate into a separatory funnel and shaking with
about 10 mL of water. Jesse observes the lower 1-bromobutane layer has a pink coloration. This is due to presence of
Br2. Suggest how Jesse can rectify this.
O Add a pinch of sodium bisulfite, NAHSO3.
O Rinse the 1-bromobutane layer with another portion of water.
Add a scoop of anhydrous CaCl2.
Add 10 ml. of cold concentrated H2SO4
Transcribed Image Text:The workup of preparation of 1-bromobutane involves pouring the distillate into a separatory funnel and shaking with about 10 mL of water. Jesse observes the lower 1-bromobutane layer has a pink coloration. This is due to presence of Br2. Suggest how Jesse can rectify this. O Add a pinch of sodium bisulfite, NAHSO3. O Rinse the 1-bromobutane layer with another portion of water. Add a scoop of anhydrous CaCl2. Add 10 ml. of cold concentrated H2SO4
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