Identify the identity of the 3 peaks options: ether, acetic acid, alcohol, and ether Potentia4.48mVLatestTimePotential200Time: 1.817200 min(min)0.0000000.0077000.0154000.0231000.0308000.0385000.0462000.0539000.06160010 0.06930011 0.07700012 0.08470013 0.09240014(mV)Potential Slope:-2.637 mV/min5.243.1.5.245.395.311505.245.241005.315.155.245.24505.315.245.240.100100150.1155000.123200185.240.1078005.15(At:0.551 Ay:8.4)165.15Time (min)175.24Peaks for: Latest Potential5.315.155.155.155.085.155.155.080.130900190.138600#3CompoundRetention Time (min)Area% Area20 0.146300210.1540000.9320.090.611Peak 10.5850.060.36220.161700Peak 21.17815.4299.0323 0.16940024Peak 30.17710025 0.18480026 0.19250027 0.20020028 0.20790029 0.21560030 0.22330O5.245.155.155.085.085.15310.23100032 0.23870033 0.2464004 0.2541000.2618006 0.2695005.155.085.085.245.0835Potential4.48 mV2.23Potential (mV)1234567 89

Peak 3 is corresponding to acetic acid. Peak 2 is corresponding to ether group. Peak 1 is…

Time Poential 200 Tere 1a700 mn minl 1000000 2 0.007700 3 0.015400 0.023100 0.030800 60.038500 7 0.046200 0.053900 9 0.061600 10 0.069300 11 0.077000 12 J0.084700 13 J0.092400 140.100100 15 0.107800 16 0.115500 17 0.123200 18 Potential ooe 67 mown 5.24 5.24 5.30 5.31 524 5.24 531 535 524 150 100 5.24 5.31 60- 5.24 5.24 5.24 515 5.15 5.24 5.31 5.15 5.15 515 5.08 515 5.15 5.08 5.24 5.15 5.15 5.08 5.08 5.15 515 2. (At0.551 Ay 8.4) Time min Pkator.Latesteental 0.130900 19 0.138600 20 0146300 21 0.154000 22 0.161700 R3 0.169400 24 0.177100 25 0.184800 26 0.192500 27 0.200200 28 0.207900 9 0.215600 0 0.223300 81 0.231000 2 0 238700 3 J0.246400 4 0.254100 50.261800 6 0.269500 %23 Compound Retention Time (min) Area % Area 0.932 0.09 061 1. Peak 1 0.585 0.06 0.36 2. Peak 2 1178 15.42 99.03 3. Peak 3 5.00 5.08 5.24 5.08 Potential 4,48 mV

Time Poential 200 Tere 1a700 mn minl 1000000 2 0.007700 3 0.015400 0.023100 0.030800 60.038500 7 0.046200 0.053900 9 0.061600 10 0.069300 11 0.077000 12 J0.084700 13 J0.092400 140.100100 15 0.107800 16 0.115500 17 0.123200 18 Potential ooe 67 mown 5.24 5.24 5.30 5.31 524 5.24 531 535 524 150 100 5.24 5.31 60- 5.24 5.24 5.24 515 5.15 5.24 5.31 5.15 5.15 515 5.08 515 5.15 5.08 5.24 5.15 5.15 5.08 5.08 5.15 515 2. (At0.551 Ay 8.4) Time min Pkator.Latesteental 0.130900 19 0.138600 20 0146300 21 0.154000 22 0.161700 R3 0.169400 24 0.177100 25 0.184800 26 0.192500 27 0.200200 28 0.207900 9 0.215600 0 0.223300 81 0.231000 2 0 238700 3 J0.246400 4 0.254100 50.261800 6 0.269500 %23 Compound Retention Time (min) Area % Area 0.932 0.09 061 1. Peak 1 0.585 0.06 0.36 2. Peak 2 1178 15.42 99.03 3. Peak 3 5.00 5.08 5.24 5.08 Potential 4,48 mV

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter34: Particle Size Determination

Section: Chapter Questions

Problem 34.10QAP

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