What is the IR and HNMRAndCNMR and mass in this example

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter20: Molecular Mass Spectrometry
Section: Chapter Questions
Problem 20.11QAP
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What is the IR and HNMRAndCNMR and mass in this example
IR Spectrum
(liquid film)
4000
100
80
3000
57
60
40
20
40
13C NMR Spectrum
(50.0 MHz, CDCI, solution)
29
80
100
DEPT CH₂ CH₂ CH
proton decoupled
200
¹H NMR Spectrum
(200 MHz, CDCI, solution)
11
10
9
138
8
2000
120
1743
1600
v (cm¹)
WW
m/e
160
M = 174 (<1%)
160 200 240 280
120
1200
7 6
800
Mass Spectrum
1
5
C8H1404
solvent
A
L
80
4
1
Final Exam
Problem 49
No significant UV
absorption above 220 nm
3
Azad Univers
40
11
2
1
rch Branch
08 (ppm)
ter of f
AL
TMS
0
8 (ppm)
Transcribed Image Text:IR Spectrum (liquid film) 4000 100 80 3000 57 60 40 20 40 13C NMR Spectrum (50.0 MHz, CDCI, solution) 29 80 100 DEPT CH₂ CH₂ CH proton decoupled 200 ¹H NMR Spectrum (200 MHz, CDCI, solution) 11 10 9 138 8 2000 120 1743 1600 v (cm¹) WW m/e 160 M = 174 (<1%) 160 200 240 280 120 1200 7 6 800 Mass Spectrum 1 5 C8H1404 solvent A L 80 4 1 Final Exam Problem 49 No significant UV absorption above 220 nm 3 Azad Univers 40 11 2 1 rch Branch 08 (ppm) ter of f AL TMS 0 8 (ppm)
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