Which of the following compounds will give an orange precipitate when reacted with 2,4 dinitrophenylhydrazine and form a silver mirror on warning with ammoniacal silver 1. nitrate? A CH;CH2CH2COCI B CH3CH2CH(CH3)CHO C CH;CH2COCH2CH D CH;CH(CH;) CH (OH) C= CH
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- (a)Which compound/s will produce an orange precipitate upon reaction with 2,4-DNPH? (b)Which compound/s will test positive towards Baeyer’s test? (c)Which compound/s will produce a brick-red precipitate upon reaction with Fehling’s reagent (CuSO4, tartrate, NaOH)? (d)Which compound/s will test positive towards the Iodoform test?a) Write out the first 3 steps only(to the tetrahedral intermediate shown) in the 6-step arrow pushing mechanism showing how ethyl propanoate is hydrolyzed in acid to form propanoic acidand ethanol. b) NaOH/H2O also serveto hydrolyze an ester; briefly explain why NaOH/H2Ois generally preferable.Suggest the most appropriate method for each of the following laboratory syntheses. Ineach case, suggest both a chromium reagent and a chromium-free reagent. butan@2@ol ¡ butan@2@one, CH3COCH2CH3
- Give the major organic product of each reaction of γ‑valerolactone with each of the given six reagents under the conditions indicated. Do not draw any byproducts formed. Reagent 1. NaOH, H2O, heat, then H+, H2O 2. (CH3)2CHCH2CH2OH (excess), H+ 3. (CH3CH2)2NH and heat 4. CH3MgI (excess), ether, then H+/H2O 5. LiAlH4, ether, then H+/H2O 6. DIBAL, toluene, low temperature, then H+/H2ODevise a synthesis of the ketone hexan-3-one, CH3CH2COCH2CH2CH3, from CH3CH2Br as the only organic starting material; that is, all the carbon atoms in hexan-3-one must come from CH3CH2Br. You may use any other neededreagents.How to prepare the Organometallic Reagents ?
- What products would you expect from the oxidation of thefollowing compounds with (i) CrO3 in aqueous acid? (ii) withPCC?(a) tert-butanol(b) cyclohexanol(c) cyclohexanoneCompelling evidence for the existence of a tetrahedral intermediate innucleophilic acyl substitution was obtained in a series of elegantexperiments carried out by Myron Bender in 1951. The key experimentwas the reaction of aqueous −OH with ethyl benzoate (C6H5COOCH2CH3)labeled at the carbonyl oxygen with 18O. Bender did not allow thehydrolysis to go to completion, and then examined the presence of alabel in the recovered starting material. He found that some of therecovered ethyl benzoate no longer contained a label at the carbonyloxygen. With reference to the accepted mechanism of nucleophilic acyl substitution, explain how this provides evidence for a tetrahedralintermediate.Explain the following observation. Ethyl 3-phenylpropanoate (C6H5CH2CH2CO2CH2CH3) reacts with electrophiles to afford ortho- and para-disubstituted arenes, but ethyl 3-phenylprop-2-enoate (C6H5CH= CHCO2CH2CH3) reacts with electrophiles to afford meta-disubstituted arenes.
- 9. Product of the reaction of nitrobenzene with sulfuric acid in the presence of oleum at 60 °C:a) o-nitro benzenesulfonic acidb) m-nitro benzenesulfonic acidc) p-nitro benzenesulfonic acidd) None of the above 10. Due to their ability to move through ducts or pipes, they are generally called fluids:a) Solidsb) Solid mixturesc) Gasesd) Liquids and gasesTo prepare butanoic acid from 1-propanol, which sequence of reagent(s) is/are best employed? a) (1) NaCN; (2) H2O; (3) [H+] b) LiAlH4 c) K2Cr2O7 in acid d) (1) PBr3; (2) NaCN; (3) H2O; (4) [H+]Which product is formed by the reaction of the compound shown with LiAlH4? a. I b. II c. III d. IV e. none of these