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- Calculate the saturation indices of the solutions described below and classify each as undersaturated, supersaturated, or in equilibrium. Saturation state with respect to: Anhydrite (CaSO4) [Ca2+] = 0.00002 mM [SO42-] = 25 mM “Amakinite” (Fe(OH)2) [Fe2+] = 0.1 mM; [OH-] = 0.0001 mM Siderite (FeCO3) [Fe2+] = 3 mM; [CO32-] = 10 mMCalculate the saturation indices of the solutions describe below and classify each as undersaturated, supersaturated, or in equilibrium. Saturation state with respect to: Anhydrite (CaSO4) [Ca2+] = 0.00002 mM [SO42-] = 25 mM “Amakinite” (Fe(OH)2) [Fe2+] = 0.1 mM; [OH-] = 0.0001 mM Siderite (FeCO3) [Fe2+] = 3 mM; [CO32-] = 10 mMWhat weight of strontium acetate containing 99% Sr(CH3COOH)2.½H2O must be used as sample in an assay according to the general method for alkali salts of organic acids if, after treatment of the ash with 50.00 ml of 0.5162 N hydrochloric acid, it is desirable to consume 30.00 ml of 0.4675 N sodium hydroxide in the back titration?
- 1. an accurately weighed chelometric standard calcium carbonate of 150 mg was used to standardize Disodium ethylenediaminetetraacetate, using the same procedure set by the monograph. The total volume of EDTA consumed was 37.5 ml . Calculate the molarity and normality of the standard solution. 2. A 0.62L of 0.072N silver nitrate was used to titrate three samples of sodium lauryl sulfate with 2500 mg,5000mg, and 6750 mg respectively. Tabulate its data, calculate the %NaCl in each sample , did any sample conformed to the official requirement?A sample is analyzed for chloride by the Volhard method. Calculate the %KCl from the following data: Wt of sample = 0.5000g; Vol of AgNO3 added = 35.00ml; M of AgNO3 = 0.1157; Vol of SCN- used for back titration = 14.71ml; M of SCN- = 0.08598; Atomic wts: Ag = 107.87, N = 14.00, Cl = 35.5, O = 16.00A 1.000-g sample containing bromide was dissolved in sufficient water to give 100.0 mL. A 50.00 mL aliquot was measured and after acidification, silver nitrate was introduced to precipitate AgBr, which was filtered, washed, and then dissolved in an ammoniacal solution of potassium tetracyanonickelate(II): Ni(CN)42- + 2AgBr(s) → 2Ag(CN)2- + Ni2+ + 2Br-Nickel ion required 11.70 mL of 0.002146 M EDTAWhat is the percentage of NaBr (102.894) in the 1.000 g sample?
- Calcium fluoride is considered as a relatively insoluble compound and therefore lime or slakedlime has been considered as a possible material to remove excess fluoride in water of boreholesin certain parts of the country. The solubility product of CaF2 is Ksp = 3 x 10 – 11 and that ofCa(OH)2 isKsp =8x10-61. How much lime can be added to the water to remove 10 mg of F- ion per litre ofborehole water?(The atomic masses are Ca: 40.08; F: 19.00; O: 16; H: 1)A 1.000-g sample containing bromide was dissolved in sufficient water to give 100.0 mL. A 50.00 mL aliquot was measured and after acidification, silver nitrate was introduced to precipitate AgBr, which was filtered, washed, and then dissolved in an ammoniacal solution of potassium tetracyanonickelate(II): Ni(CN)42- + 2AgBr(s) → 2Ag(CN)2- + Ni2+ + 2Br- The liberated nickel ion required 11.70 mL of 0.002146 M EDTA. Calculate mmol Ni in the 50.00 mL aliquot. Calculate mmol Br- in the 50.00 mL aliquot. Calculate the percentage of NaBr (102.894) in the 1.000 g sample.A 1.000-g sample containing bromide was dissolved in sufficient water to give 100.0 mL. A 50.00 mL aliquot was measured and after acidification, silver nitrate was introduced to precipitate AgBr, which was filtered, washed, and then dissolved in an ammoniacal solution of potassium tetracyanonickelate(II): Ni(CN)42- + 2AgBr(s) → 2Ag(CN)2- + Ni2+ + 2Br- The liberated nickel ion required 11.70 mL of 0.002146 M EDTA The other 50.00 mL remaining solution was also analyzed for its Br- content by potentiometry using a metallic electrode of the second kind. Ecell recorded in running the solution using the potentiometric set-up was Ecell = 0.0286 V. (E0Ag/AgBr = 0.095 V) g) Compute for Eind. h) Compute pBr in the 50.00 mL aliquot. i) Compute for % NaBr ( in the potentiometric technique). j) Calculate the error between the obtained % NaBr fr the EDTA titration technique and the % NaBr from the potentiometric technique.
- 1000 litres of hard H2O is softened by zeolite process. The zeolite was regenerated by passing 20 litres of sodium chloride solution containing 1500 mg/lit. of NaCl. Calculate hardness of H2O?a.) What are the primary standard substances used in the adjustment of thiosulfate solutions?b.) When should starch indicator be added in iodometric titration? Explain why.c.) Since 31.4 mL of 0.10 N Na2S2O3 solution is consumed in the iodometric determination of copper at a weight of 2,000 g taken from a copper-containing material, find the percentage of copper in the sample (Cu: 63.5 gmol-1).The accompanying data (1.00-cm cells) were obtained for the spectrophotometric titration 10.00 mL of Pd(II) with 2.44 10-4 M Nitroso R(O. W Rollins and M. M. Oldham, Anal. chem .,1971, 43, 262, DOI: 10.1021/ac60297a026). Calculate the concentration of the Pd(II) solution, given that the ligand-to-cation ratio in the colored product is 2:1