. A 1.6394-g sample of limestone taken from Sinuhutan Cave in Brgy. Onop, Miagaowas analyzed for Fe, Ca, and Mg. The iron was determined as Fe203, that yielded a weightof 0.0572 g. The calcium content was isolated as CaSO4, with a precipitate of 1.5804 g,and Mg was reported as Mg2P207 weighing 0.0726 g. report the amount of Fe, Ca, and Mgin the limestone sample as %w/w Fe203, %w/w Cao, and %w/w MgO.

A numerical problem based on inorganic chemistry, which is to be accomplished.

Answered: .A 1.6394-g sample of limestone taken…

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter12: Gravimetric Methods Of Analysis

Section: Chapter Questions

Problem 12.20QAP

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A. 1.4639 g sample of limestone was analyzed for Fe, Ca and Mg. The iron was determined as Fe2O3, yielding 0.0357 g Calcium was isolated as CaSO4, yileding a precipitate of 1.4058 g and Mg was isolated as 0. 0627 g of MgP2O7. Report the amount of Febas %w/w Fe2O3, Ca as %w/w CaO and Mg in the limestone sample as % w/w MgO
To analyze the amount of iron (Fe; Mw = 55.85 g/mol) contained in an ore sample, the sample was digested with acid and diluted to 50 mL with water. This solution was then treated with 25.00 mL of 0.2922 M EDTA. The excess EDTA was back titrated with 6.47 mL of 0.0843 M Zn2+ to reach the equivalence point. How many grams of Fe contained in the ore sample?
A 0.7336-g sample of an alloy that contains copper and zinc is dissolved in 8 M HCl and diluted to 100 mL in a volumetric flask. In one analysis, the zinc (At. Mass = 65.38 g/mol) in a 25.00-mL portion of the solution is precipitated as ZnNH4PO4, and isolated as Zn2P2O7 (FM = 304.70g/mol), yielding 0.1163 g. The copper (At. Mass = 63.55 g/mol) in a separate 25.00-mL portion of the solution is treated to precipitate CuSCN (121.63 g/mol), yielding 0.2383 g. Calculate the %w/w Zn and the %w/w Cu in the sample.
A 1.1324 g sample of magnetite ore was dissolved in concentrated HCl to give a solution that contained a mixture of Fe2+ and Fe3+. Nitric acid was added and the solution was boiled for a few minutes, which converted all of the iron to Fe3+. The Fe3+ was then precipitated as Fe2O3*xH2O by addition of NH3. After filtration and washing, the residue was ignited at a high temp to give 0.5394 g of pure Fe2O3. What is the percent Fe and the percent Fe3O4 in the sample?
A 5.70 g iron ore was dissolved in concentrated HCl. After the dissolution, the resulting solution was made basic by adding 6.0 M NaOH slowly until the solution is slightly turbid. Urea was then added and the solution was heated for 3 hours. The precipitate was filtered using an ashless filter paper and ignited to form Fe2O3 (159.69 g/mol). The mass of precipitate is 2.1 g. Find the % Fe3O4 (231.54 g/mol) in the iron ore sample.
1,5419 g of magnetite (Fe3O4) ore; Fe+2 and Fe + 3 in concentrated HCL to form a mixtureit's unraveling. Adding HNO3 to all Fe +2s Fe +3 e and Fe+3 s NH, addingwith Fe(OH)3, precipitating into. Sediment in the form of Fe3O4 after necessary operationsand 0.8525 g. Calculate the percentage of Fe3O4 in the sample.
A 0.7352g sample of ore containing Fe3+, Al3+ and Sr2+ was dissolved and made up to 500.00 mL. The analysis of metals was performed by a chemistry using complexation volumetry. Initially, an aliquot of 50.00 mL had its pH adjusted to 1.0 and titrated with a standard solution of EDTA 0.02145 mol/L, requiring 6.95 mL to reach the end point. Subsequently, another 25.00 mL aliquot was buffered at pH=5 and titrated with the same EDTA solution, requiring 6.24 mL to reach the end point. Finally, a third aliquot of 25.00 mL was titrated at pH=11, requiring 11.10 mL of the same EDTA solution to complete the titration. Determine the percentage of each of the metals in the sample Given the molar masses: Fe=55.845 g/mol; Al=26.982 g/mol and Sr=87.620 g/mol.
What is the percentage of Nickel in an ore if, when analyzed by the cyanide method, 20.00mL of KCN solution (containing 1.00mmol of AgNO3 per milliliter) are used? Wt of sample used = 0.2500g
A Chemist collected a 0.4891-g sample of an ore for Fe determination by a redox titration with K2Cr2O7.The ore was carefully crushed prior to weighing and dissolved in HCl and using a Jones reductor the ironin the sample was brought into the +2 oxidation state. After titration with diphenylamine sulfonic acid,itrequired 36.92 mL of 0.02153 M K2Cr2O7 to reach the end point. Show your solution why 77.86% is the iron content of the ore as %w/w Fe2O3.
A Chemist collected a 0.4891-g sample of an ore for Fe determination by a redox titration with K2Cr2O7.The ore was carefully crushed prior to weighing and dissolved in HCl and using a Jones reductor the ironin the sample was brought into the +2 oxidation state. After titration with diphenylamine sulfonic acid,itrequired 36.92 mL of 0.02153 M K2Cr2O7 to reach the end point. Calculate the iron content of the ore as%w/w Fe2O3
(a) What is the percentage of MnO2 in a pyrolusite ore if a sample weighing 0.4000g is treated with 0.6000g of pure H2C2O4•2H2O and dilute H2SO4 and after reduction has taken place (MnO2 + H2C2O4 + 2H+→ Mn2++ 2CO2 + 2H2O), the excess oxalic acid requires 26.26ml of 0.1000N KMnO4 for titration? (b) If pure As2O3 were used instead of oxalic acid, how many grams would be required in order for the other numerical data to remain the same?
(a) What is the percentage of MnO2 in a pyrolusite ore if a sample weighing 0.4000 g is treated with a 0.6000 g of pure H2C2O4.2H20 and dilute H2SO4 and after reduction has taken place (MnO2 + H2C2O4 + 2H+ Mn2+ + 2CO2 + 2H2O), the excess oxalic acid requires 26.26 mL of 0.1000 N KMNO4 for titration? (b) If pure As2O3 were used instead of oxalic acid, how many grams would be required in order for the other numerical data to remain the same?

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