0:08 AM Thu Mar 23 Problem 33 of 23 Br2 (1 equiv) Draw the product of the reaction shown below. Ignore inorganic byproducts. FeBr3 Select to Draw @ 66% Q Submit
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- please provide the machanisms of 1a, 1e, 1fFor 20.7 the solutions for part c and d dont seem right. Shouldn't reacting with 1 eq of H2 just take away the C=C bond and not the C=O bond. (H2 reduces C=C selectively to form a ketone according to page 738. Also the both the C=C and C=O bond should be reduced if excess H2 is usedTaking Ka for acidic acid as 1.8 x 10-5, calculate H3O+ , using the known concentraions of acidic acid and soudium acecate contained in reaction mixtures 1 and 4. Reaction mixture time (s) Acidic acid concentration (mol/L) sodium acetate concentration (mol/L) calculated H3O+ concentration 1 237 0 1 x 10 -5 4 236 1 x 10 -4 1 x 10 -5
- I’m currently trying to write a lab report for the synthesis of dimolybdenum tetraacetate [Mo2(O2CCH3)4] from the reaction of molybdenum hexacarbonyl, Mo(CO)6 in glacial acetic acid and acetic anhydride under a nitrogen atmosphere, involving the difficult formation of a quadruple bond and requires high heat and long reaction time (approximately 20 hours). But these are the question I’m stumped on: 1. Why need the reaction be done under nitrogen? We also added dichlorobenzene and hexanes during the reaction. 2. Explain the purpose of dichlorobenzene and hexanes. 3. Why does the reaction take 20 hrs?Tunicates are marine animals that are called "sea squirts" because when they are taken out of water, they tend to contract and expel seawater. Lepadiformine is a cytotoxic agent (toxic to cells) isolated from a marine tunicate. During a recent synthesis of lepadiformine, the investigators observed the formation of an interesting by-product (3) while treating diol 1 with a reagent similar in function to PBr3 (J. Org. Chem. 2012, 77, 3390–3400):SHOW COMPLETE SOLUTIONS Q3. Which isolate has A260/280 ratio of above 2.0?
- Provide details about the reaction workup. 4,4'-DIBROMOBIPHENYL [Biphenyl, 4,4'-dibromo-] Submitted by Robert E. Buckles and Norris G. Wheeler1. Checked by R. S. Schreiber, Wm. Bradley Reid, Jr., and Robert W. Jackson. 1. Procedure In a 15-cm. evaporating dish is placed 15.4 g. (0.10 mole) of finely powdered biphenyl (Note 1). The dish is set on a porcelain rack in a 30-cm. desiccator with a 10-cm. evaporating dish under the rack containing 39 g. (12 ml., 0.24 mole) of bromine. The desiccator is closed, but a very small opening is provided for the escape of hydrogen bromide (Note 2). The biphenyl is left in contact with the bromine vapor for 8 hours (or overnight). The orange solid is then removed from the desiccator and allowed to stand in the air under a hood for at least 4 hours (Note 3). At this point, the product weighs about 30 g. and has a melting point in the neighborhood of 152°. The crude 4,4'-dibromobiphenyl is dissolved in 75 ml. of benzene, filtered, and cooled to 15°.…Solution:- 3. Determine the amount, in of a (2.20 M s olution of dichloromethane needed to completely react with 15.72g cyclohexene to give 1,2-dibromocuclohexanw. Assume 12% excess is needed in order to react completely. a . How much 1,2 -dibromocyclohexane would theoretically be produced ? c. How many ML of the 2.20 M Br2 solution are required?In light of your answer to Problem 30-40, explain why a mixture of products occurs in the following reaction:
- A student attempted to prepare 1-chlorobutane by mixing 1-butanol with NaCl in acetone. Was the student succesful? Explain.Make a table of the physical properties (molar mass, MPT, BPT density and mass used/needed) for the reduction of benzophenone lab reactions. (bezhydrol is the product of reaction). Plz do fast asap, urgent.Prove that the Keq for the reaction between Pb2+ and HF is 12.4. (Ksp, PbF2 = 6.76 x 10-4 and dissociation constant of HF is 3.7 x 10-8)