1. Phoa pyridine1. Provide the major products of each reaction sequence below.1. PhBr, Pd(PPh,), Cul, NEt,2. LIAIH,HO,3. Dess Martin Periodinane4. CH,CH,CO,Me, LDA then H,01.2. Pd(PPhala, Na;CO,, PhBrPh3. lz. AGOAC4. КОН, Н.оOMe5. TSOH,1. Ti(OiPr)4. (+)-DET, IBUOOH(stop at 50% conversion,remove reacted product)PhMeMe2. NaH then Mel3. O, then Me,SOH4. Me,SICH,MgBr then H,SO.1. CH;0, NH3, NH,CI2. CBZCI, Na,CO,3. NH,OH then H,SO,1. PhOCI pyridine2. Bu, SnH, AIBN, A3. Cp,TICI, Me,AI4. H,05. NABH, CeCl, MeOH

“Since you have asked multiple question, we will solve the first question for you. If youwant any…

Answered: 1. Provide the major products of each…

1. Provide the major products of each reaction sequence below. 1. PhBr, Pd(PPh,), Cul, NEt, 2. LIAIH, 3. Dess Martin Periodinane 4. CH,CH,CO,Me, LDA then H,0

Organic Chemistry: A Guided Inquiry

2nd Edition

ISBN:9780618974122

Author:Andrei Straumanis

Publisher:Andrei Straumanis

Chapter13: Substitution

Section: Chapter Questions

Problem 59CTQ

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Concept explainers

Alkanes and Cycloalkanes

Alkanes are saturated organic compounds which are made up of C and H atoms. Alkanes have the general formula of CnH2n+2. Alkane contains sp3 hybridized carbon atoms with four sigmas (σ) bonds & every hydrogen atom is connected with one of the carbon atoms. The size of the alkane could be determined by the number of carbon atoms located in it.

Question

1. Phoa pyridine
1. Provide the major products of each reaction sequence below.
1. PhBr, Pd(PPh,), Cul, NEt,
2. LIAIH,
HO,
3. Dess Martin Periodinane
4. CH,CH,CO,Me, LDA then H,0
1.
2. Pd(PPhala, Na;CO,, PhBr
Ph
3. lz. AGOAC
4. КОН, Н.о
OMe
5. TSOH,
1. Ti(OiPr)4. (+)-DET, IBUOOH
(stop at 50% conversion,
remove reacted product)
Ph
Me
Me
2. NaH then Mel
3. O, then Me,S
OH
4. Me,SICH,MgBr then H,SO.
1. CH;0, NH3, NH,CI
2. CBZCI, Na,CO,
3. NH,OH then H,SO,
1. PhO
CI pyridine
2. Bu, SnH, AIBN, A
3. Cp,TICI, Me,AI
4. H,0
5. NABH, CeCl, MeOH

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