102 4000 100 80 60 40 20 2089 IR Spectrum (quid fam) % of base peak 3000 63 65 83 40 80 13C NMR Spectrum (50.0 MHz. CDCI, solution) proton coupled proton decoupled 200 ¹H NMR Spectrum (200 MHz. CDCI, solution) 10 9 8 2000 V (cm¹) M 98/100/102 120 m/e 160 160 7 m 1600 200 120 1200 6.0 5.8 ppm I 6 800 Mass Spectrum 240 680 C2H4Cl2 280 expansions سلللم solvent 1 L 80 1 22 2.0 ppm 5 4 Problem 13 No significant UV absorption above 220 nm 3 40 2 119 08 (ppm) TMS 1 1 1 0 8 (ppm) -

102 4000 100 80 60 40 20 2089 IR Spectrum (quid fam) % of base peak 3000 63 65 83 40 80 13C NMR Spectrum (50.0 MHz. CDCI, solution) proton coupled proton decoupled 200 ¹H NMR Spectrum (200 MHz. CDCI, solution) 10 9 8 2000 V (cm¹) M 98/100/102 120 m/e 160 160 7 m 1600 200 120 1200 6.0 5.8 ppm I 6 800 Mass Spectrum 240 680 C2H4Cl2 280 expansions سلللم solvent 1 L 80 1 22 2.0 ppm 5 4 Problem 13 No significant UV absorption above 220 nm 3 40 2 119 08 (ppm) TMS 1 1 1 0 8 (ppm) -

Organic Chemistry

8th Edition

ISBN:9781305580350

Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Chapter13: Nuclear Magnetic Resonance Spectroscopy

Section: Chapter Questions

Problem 13.28P

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